Preparation and Characterization of Kenaf and Oil Palm Nanocellulose by Acid Hydrolysis Method

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Acid hydrolysis method become one of the attention among researcher to produce high degree nanocellulose. Integration of sonication process was used to stir and mix particles in an element for different stages. This paper revealed the surface morphology and crystallinity index of two organic plant that were kenaf and oil palm nanocellulose. Characterization of the nanocellulose were identified by 2 techniques; (1) field emission scanning electron microscope (FESEM) that provides surface morphology and elemental information of the element, (2) x-ray diffraction (XRD) for phase identification of materials crystallinity. The result showed that the properties of nanocellulose increase after sonication method have been integrated.

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Materials Science Forum (Volume 1010)

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495-500

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September 2020

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© 2020 Trans Tech Publications Ltd. All Rights Reserved

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[1] Srndovic, J. S. (2011). Interactions between Wood Polymers in Wood Cell Walls and Cellulose/Hemicellulose Biocomposites. Department of Chemical and Biological Engineering (Vol. Doctor of).

Google Scholar

[2] Morán, J. I., Alvarez, V. A., Cyras, V. P., & Vázquez, A. (2008). Extraction of cellulose and preparation of nanocellulose from sisal fibers. Cellulose, 15(1), 149–159.

DOI: 10.1007/s10570-007-9145-9

Google Scholar

[3] Trache, D., Hussin, M. H., Haafiz, M. K. M., & Thakur, V. K. (2017). Recent progress in cellulose nanocrystals: sources and production. Nanoscale, 9(5), 1763–1786.

DOI: 10.1039/c6nr09494e

Google Scholar

[4] Siró, I., & Plackett, D. (2010). Microfibrillated cellulose and new nanocomposite materials: a review. Cellulose.

DOI: 10.1007/s10570-010-9405-y

Google Scholar

[5] Wulandari, W. T., Rochliadi, A., & Arcana, I. M. (2016). Nanocellulose prepared by acid hydrolysis of isolated cellulose from sugarcane bagasse. In IOP Conference Series: Materials Science and Engineering (Vol. 107, No. 1, p.012045). IOP Publishing.

DOI: 10.1088/1757-899x/107/1/012045

Google Scholar

[6] Surip, S. N., Wan Jaafar, W. N. R., Azmi, N. N., & Anwar, U. M. K. (2012). Microscopy observation on nanocellulose from kenaf fibre. In Advanced Materials Research (Vol. 488, pp.72-75). Trans Tech Publications.

DOI: 10.4028/www.scientific.net/amr.488-489.72

Google Scholar

[7] Lani, N. S., Ngadi, N., Johari, A., & Jusoh, M. (2014). Isolation, characterization, and application of nanocellulose from oil palm empty fruit bunch fiber as nanocomposites. Journal of Nanomaterials, 2014, 13.

DOI: 10.1155/2014/702538

Google Scholar

[8] Rahimi Kord Sofla, M., Brown, R. J., Tsuzuki, T., & Rainey, T. J. (2016). A canofibres extracted from bagasse using acid and ball milling methodsomparison of cellulose nanocrystals and cellulose n. Advances in Natural Sciences: Nanoscience and Nanotechnology, 7(3).

DOI: 10.1088/2043-6262/7/3/035004

Google Scholar

[9] Surip, S. N., Wan Jaafar, W. N. R., Azmi, N. N., & Anwar, U. M. K. (2012). Microscopy Observation on Nanocellulose from Kenaf Fibre. Advanced Materials Research, 488–489(March 2012), 72–75.

DOI: 10.4028/www.scientific.net/amr.488-489.72

Google Scholar

[10] Li, Q., Ng, W. T., & Wu, J. C. (2014). Isolation, Characterization and Application of a Cellulose- degrading Strain Neurospora crassa S1 from Oil Palm Empty Fruit Bunch. Microbial Cell Factories, 13(157), 1–8.

DOI: 10.1186/s12934-014-0157-5

Google Scholar

[11] Surip, S. N., Bonnia, N. N., Anuar, H., Hassan, N. A., & Yusof, N. M. (2012). Nanofibers from oil palm trunk (OPT): Preparation & chemical analysis. ISBEIA 2012 - IEEE Symposium on Business, Engineering and Industrial Applications, 809–812.

DOI: 10.1109/isbeia.2012.6423003

Google Scholar

[12] Y., Lee, H. V, & Hamid, S. B. A. (2016). Preparation of Cellulose Nanocrystals Bio-Polymer From Agro- Industrial Wastes: Separation and Characterization. Polymers & Polymer Composites, 24(9), 719–728.

DOI: 10.1177/096739111602400907

Google Scholar

[13] Kallel, F., Bettaieb, F., Khiari, R., García, A., & Bras, J. (2016). Isolation and structural characterization of cellulose nanocrystals extracted from garlic straw residues. Industrial Crops & Products, 87, 287–296.

DOI: 10.1016/j.indcrop.2016.04.060

Google Scholar

[14] Bast, K. (2009). Chemical composition, crystallinity, and thermal degradation of bleached and unbleached kenaf bast, 4, 626–639.

Google Scholar

[15] Li, Q., Ng, W. T., & Wu, J. C. (2014). Isolation, Characterization and Application of a Cellulose- degrading Strain Neurospora crassa S1 from Oil Palm Empty Fruit Bunch. Microbial Cell Factories, 13(157), 1–8.

DOI: 10.1186/s12934-014-0157-5

Google Scholar

[16] Fahma, F., & Iwamoto, S. (2010). Isolation, preparation, and characterization of nanofibers from oil palm empty-fruit-bunch ( OPEFB ), 977–985.

DOI: 10.1007/s10570-010-9436-4

Google Scholar