Synthesis of Fluorine-Containing Organic Silane Reagent
Organic silane perfluorinated octyl sulfonic acid amide is synthesized by compounding aminosilane (N-(β-aminoethyl)-γ-aminopropyl trimethoxy silane) and perfluorinated octyl sulfonic acid fluoride. The results show that the product yield of 88% is achieved when the ratio of perfluorinated octyl sulfonic acid fluoride and aminosilane is maintained at 1:1.1 at 50°C for 2 hours.
Hyungsun Kim, JienFeng Yang, Tohru Sekino and Soo Wohn Lee
R. Weng et al., "Synthesis of Fluorine-Containing Organic Silane Reagent", Materials Science Forum, Vols. 620-622, pp. 599-602, 2009