ZnO/SiO2 Nanocomposite Cryogels Prepared by Vacuum Freeze Drying

Abstract:

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In recent years, ZnO/SiO2 nanocomposite thin films have attracted much attention for a wide range of device applications based on their specific optical and electrical properties. Traditionally, the ZnO/SiO2 nanocomposites were prepared at the form of thin film because the ZnO/SiO2 nanocomposite gels are difficult to synthesize. Therefore, in the present study, a novel route of the mixed ZnO/SiO2 nanocomposite cryogels were prepared by sol-gel technology and dried by vacuum freeze drying. The wet gels were synthesized by co-precursor method with the precursors containing tetraethoxysilane [Si(OC2H5)4,TEOS] and zinc acetate [Zn(CH3COO)2.2H2O]. After vacuum freeze drying, the nanocomposites were annealed at different temperature. The properties of the resulting ZnO/SiO2 nanocomposite cryogels were characterized using Scanning Electron Microscopy (SEM), nitrogen absorption/desorption isotherms, thermogravimetric and differential scanning calorimeter (TG-DSC).

Info:

Periodical:

Materials Science Forum (Volumes 663-665)

Edited by:

Yuan Ming Huang

Pages:

1242-1246

DOI:

10.4028/www.scientific.net/MSF.663-665.1242

Citation:

L. F. Su et al., "ZnO/SiO2 Nanocomposite Cryogels Prepared by Vacuum Freeze Drying", Materials Science Forum, Vols. 663-665, pp. 1242-1246, 2011

Online since:

November 2010

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Price:

$35.00

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