Structural and Mechanical Properties of Milled Si3N4/CNTs Composites by Spark Plasma Sintering Method

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Multiwall carbon nanotubes were dispersed with a concentration of 3wt% in silicon nitride ceramic host. A high efficiency attritor mill has been used for an effective dispersion of the filler phase in the matrix. In this work we have developed a spark plasma sintering process (SPS) suitable to consolidate and tailor the microstructure of CNT-reinforced silicon nitride-based ceramic composites. Mechanical measurements, micro-indentation investigations of the hardness and fracture toughness have been performed. Scanning electron microscopy has been involved in order to reveal the microstructure of the resulting composites.

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31-36

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November 2012

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