Thermal Stability of Nanocrystalline Grain Size in Ternary Fe-Base Alloys

Article Preview

Abstract:

We report recent research in our laboratory on the thermal stabilization of nanocrystalline binary alloys with ternary additions. Fe-Cr and Fe-Ni alloys with the ternary addition of Zr are studied. The thermal stability of these nanocrystalline alloys, prepared by mechanical alloying of powders, is studied by XRD, TEM and hardness as a function of annealing temperature. The relative importance of thermodynamic or kinetic stabilization in various temperature ranges is discussed for the different alloys. In agreement with our recent model for thermodynamic stabilization, it is found that Zr solute additions are more effective in stabilizing the nanocrystalline grain size in the Fe-Cr than in the Fe-Ni system.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

341-344

Citation:

Online since:

March 2013

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2013 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] K. Boylan, D. Ostrander, U. Erb, G. Palumbo, and K. T. Aust: Scripta Metall. Mater. 25(1991)2711.

Google Scholar

[2] A. Michels, C. C. Krill, H. Ehrhardt, R. Birringer, D. T. Wu: Acta Mater. 47 (1999) 2143

Google Scholar

[3] J. Weissmuller: J. Mater. Res. 9 (1994) 4

Google Scholar

[4] R. Kirchheim: Acta Mater. 50(2002) 413.

Google Scholar

[5] J. R. Trelewicz and C. A. Schuh: Phy. Rev.B 79 (2009) 094112.

Google Scholar

[6] M. Saber, H. Kotan, C. C. Koch, and R. O. Scattergood, A predictive model for thermodynamic stabilization of grain size, submitted 2012.

Google Scholar

[7] H. Kotan, M. Saber, C. C. Koch, and R. O. Scattergood, Mater. Sci. Engr. A: 552 (2012) 310.

Google Scholar

[8] H. Kotan, KA. Darling, M. Saber, C. C. Koch, RO. Scattergood: Effect of zirconium on grain growth and mechanical properties of a ball-milled nanocrystalline FeNi alloy, submitted 2012.

DOI: 10.1016/j.jallcom.2012.10.179

Google Scholar

[9] H. Kotan, KA. Darling, M. Saber, CC. Koch, RO. Scattergood: An in situ experimental study of grain growth in a nanocrystalline Fe91Ni8Zr1 alloy, submitted 2012.

DOI: 10.1007/s10853-012-7002-1

Google Scholar

[10] M. Saber, H. Kotan, CC. Koch, RO. Scattergood, Materials Science and Engineering A, 556 (2012) 664-670.

Google Scholar

[11] K.A. Darling, B.K. VanLeeuwen, C.C. Koch, R.O. Scattergood, Materials Science and Engineering: A, 527 (2010) 3572-3580.

DOI: 10.1016/j.msea.2010.02.043

Google Scholar

[12] M. Saber, C. C. Koch, R. O. Scattergood, In prepration.

Google Scholar