Preparation and Research of α-Fe/Montmorillonite Magnetic Material

Cheng Cheng Shi; Long Gui Peng; Zhi Wang

doi:10.4028/www.scientific.net/MSF.809-810.433

Paper Titles

BPW91 Method Used in Analyzing Electronic Structures and Magnetic Properties of Ni_n (2-13) Clusters
p.406

Study on the Development of Pretreatment Processes of Electroless Nickel Plating on Al Alloy Surface
p.412

First-Principle Studies of a High Entropy Solid Solution of AlCoCrCuFeNi_x with Different Mole Fractions of Ni
p.419

Electroless Fabrication of Nd-Fe-B/α-Fe Heterostructured Composite Magnets and their Magnetic Properties
p.426

Preparation and Research of α-Fe/Montmorillonite Magnetic Material
p.433

Effects of Ni/Co Metal Binder Phase on Mechanical Properties of Ti(C,N)-Based Cermets
p.438

Electrolytic Hydriding of La(Fe, Si)₁₃ Based Materials and its Magnetocaloric Effect
p.443

Effects of Duration on Wear Rate of a PTFE Composite
p.451

Microstructural Control of Al/Si Composites by Area-Selectively Liquid-Phase-Sintering Method
p.459

HomeMaterials Science ForumMaterials Science Forum Vols. 809-810Preparation and Research of α-Fe/Montmorillonite...

Preparation and Research of α-Fe/Montmorillonite Magnetic Material

Abstract:

α-Fe/montmorillonite (MMT) magnetic material was successfully prepared by the in-situ pillared-reduction method. The composite material was characterized by X-ray diffraction (XRD), laser particle size analyzer and other instruments. The magnetic property was researched by saturation magnetization. The results showed that: when 0.1mol/L hydroxyl-Fe was added as pillared agent, hydroxyl-Fe and cation of the MMT exchanged, leading to the inter-layer spacing expanded to 1.41nm and reached saturated pillared point. MMT interlayer hydroxyl-Fe was completely restored to α-Fe grains of 116nm when reducing agent was 0.2mol/L and produced α-Fe/MMT composite material. The average particle size of the composite was 5.529μm, the specific saturation magnetization was 0.812emu/g (9×10³A/moutside magnetic field) and exhibited ferromagnetism.

You might also be interested in these eBooks

2014 China Functional Materials Technology and Industry Forum

View Preview

Info:

Periodical:

Materials Science Forum (Volumes 809-810)

Pages:

433-437

DOI:

https://doi.org/10.4028/www.scientific.net/MSF.809-810.433

Citation:

Cite this paper

Online since:

December 2014

Authors:

Cheng Cheng Shi*, Long Gui Peng, Zhi Wang

Keywords:

Hydroxyl-Fe, In Situ Pillared-Reduction, Magnetic Property, Mmt

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

* - Corresponding Author

References

[1] S.G. Zhang, Z.Y. Xie, S.H. Shen et al. Progress of High-level Development Bentonite. Chinese Non-mentalic Mining Industry Herald. (2002), No. 1, pp.17-20. (In Chinese).

Google Scholar

[2] Y. M. LI, L. H. WEN, Y. LIU et al. Photocatalytic Degradation of Orange(2) by Fe Containing Pillared Bentonites. Journal of Functional Materials, Vol. 36 (2005), No. 6, pp.874-880.

Google Scholar

[3] H. JIANG, L. B. LIAO and S. P. WANG. Adsorption of Arsenic on Fe Oxyhydroxide- -montmorillonite Complex. Geochimica, Vol. 31(2002), No. 6, pp.593-601.

Google Scholar

[4] Z. Z. TAI, W. S. LIU, J. C. TANG et al. Nanocrystallization and Soft Magnetic Properties of Amorphous Fe86Zr7B6Cul Ribbons Annealed by Hot Isothermal Pressing. Journal of Central South University. Vol. 41(2010), No. 2, pp.460-463. (In Chinese).

Google Scholar

[5] P. YUAN, D. YANG, Q. TAO et al. Investigation on the Delaminated Iron-pillared Mont- morillonite Synthesized by Base-hydrolyzed Fe(Ⅲ) Nitrate Method. Mineral Rock Geochemistry Bulletin. Vol. 26(2007), No. 2, pp.112-114. (In Chinese).

Google Scholar

[6] G. Z. REN, Z. H. LI and B. L. HE. The Immobilization of Urease on Magnetic Chitosan Microspheres. Exchange and Adsorption. Vol. 16(2000), No. 2, pp.304-310. (In Chinese).

Google Scholar

[7] Y. WANG. Preparation and Study on Properties of Patterned BiFeO3 Thin Films. (MS., Shaan xi University of Science and Technology, China 2011), pp.45-46. (In Chinese).

Google Scholar