Preparation of BN Coating on KD-II Silicon Carbide Fiber by Dip-Coating Process

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Boron nitride (BN) coating on KD-II silicon carbide fiber was prepared from boric acid and urea by a 4-circle dip-coating process. SiCf/SiC composites were prepared from the precursor LPVCS by a HP(heat pressure) assisted PIP(precursor infiltration and pyrolysis) process. The microstructure and crystal structure of the coatings were characterized by SEM and XRD. XPS was adapted to analysis the composition and contents of different elements on the surface of BN coating. The influence of dip-coating process to the fibers was studied by the monofilament strength test. As the results, the monofilament strengths of the dip-coated fibers decreased firstly and increased subsequently. The strengths were slightly higher (3.4%) than the original fiber after 4 circles. The average flexural strength and fracture toughness of the composites with BN coating are respectively 290.8 MPa and 12.09 MPa⋅m1/2, while those of composites without coating are 144.1 MPa and 6.72 MPa⋅m1/2, respectively.

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April 2015

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© 2015 Trans Tech Publications Ltd. All Rights Reserved

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