Fabrication of SiCf/SiC Composite with In Situ Grown SiC Nanowire by Polymer and Infiltration Pyrolysis Process

Article Preview

Abstract:

SiC nanowires were in-situ grown in SiC fiber fabrics by chemical vapor deposition (CVD) process via pyrolysis of polycarbosilane (PCS) at 1300°C and 1400°C, respectively. Then SiCf/SiC composites were fabricated with the fabrics by polymer and infiltration pyrolysis (PIP) process. Single-filament tensile strengths of the SiC fibers heat treated at different temperature were measured. It was indicated that the mechanical property of the KD-ISiC fiber significantly degenerated above 1100°C, especially at 1400°C. Nevertheless, the prepared SiCf/SiC composite with in-situ grown SiC nanowires exhibited good mechanical performance, suggesting that the SiC nanowire is an effective reinforcement for the SiCf/SiC composite.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

32-37

Citation:

Online since:

March 2016

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2016 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] H. Yu, X. Zhou, W. Zhang, H. Peng, C. Zhang, Mechanical behavior of SiCf/SiC composites with alternating PyC/SiC multilayer interphases, Mater. Des. 44 (2013) 320-324.

DOI: 10.1016/j.matdes.2012.07.073

Google Scholar

[2] E. Buet, C. Sauder, S. P. Brender, R. Gadiou, C. Vix-Guterl, Influence of chemical and physical properties of the last generation of silicon carbide fibres on the mechanical behaviour of SiC/SiC composite, J. Eur. Ceram. Soc. 32 (2012) 547-557.

DOI: 10.1016/j.jeurceramsoc.2011.09.023

Google Scholar

[3] H. Yu, X. Zhou, W. Zhang, H. Peng, C. Zhang, Z. Huang, Mechanical properties of 3D KD-I SiCf/SiC composites with engineered fiber-matrix interfaces, Compos. Sci. Technol. 71 (2011) 699-704.

DOI: 10.1016/j.compscitech.2011.01.014

Google Scholar

[4] H. Liu, H. Cheng, J. Wang, R. Che, G. Tang, Q. Ma, Microstructural investigations of the pyrocarbon interphase in SiC fiber-reinforced SiC matrix composites, Mater. Lett. 63 (2009) 2029-(2031).

DOI: 10.1016/j.matlet.2009.06.040

Google Scholar

[5] K. Sun, J. Yu, C. Zhang, X. Zhou, In situ growth carbon nanotube reinforced SiCf/SiC composite, Mater. Lett. 66 (2011) 92-95.

DOI: 10.1016/j.matlet.2011.07.105

Google Scholar

[6] Y. Katoh, T. Nozawa, L. Snead, Mechanical properties of thin pyrolytic carbon interphase SiC-matrix composites reinforced with near-stoichiometric SiC fibers,J. Am. Ceram. Soc. 88 (2005) 3088-3095.

DOI: 10.1111/j.1551-2916.2005.00546.x

Google Scholar

[7] H. Wang, X. Zhou, J. Yu, Y. Cao, R. Liu, Fabrication of SiCf/SiC composites by chemical vapor infiltration, Mater. Lett. 64 (2010) 1691-1693.

DOI: 10.1016/j.matlet.2010.05.013

Google Scholar

[8] K. Shimoda, J. S Park, T. Hinoki, A. Kohyama. Microstructural optimization of high-temperature SiC/SiC composites by NITE process, J. Nucl. Mater. 386-388 (2009) 634-638.

DOI: 10.1016/j.jnucmat.2008.12.234

Google Scholar

[9] S. Zhao, X. Zhou, H. Yu, H. Wang, Y. Wu, Q. Huang, Z. Zhu, Z. Huang, Compatibility of PIP SiCf/SiC with LiPb at 700 ℃, Fusion Eng. Des. 85 (2010) 1624-1626.

DOI: 10.1016/j.fusengdes.2010.04.060

Google Scholar

[10] S. Zhao, X. Zhou, J. Yu, P. Mummery, Effect of heat treatment on microstructure and mechanical properties of PIP-SiC/SiC composites, Mater. Sci. Eng. A 559 (2013) 808–811.

DOI: 10.1016/j.msea.2012.09.027

Google Scholar

[11] Y. J, X. Zhou, H. Wang, S. Zhao, Y. Wu, Q. Huang, Z. Zhu, Z. Huang, 2D SiC/SiC composite for flow channel insert (FCI) application, Fusion Eng. Des. 85 (7-9) (2010) 1693-1696.

DOI: 10.1016/j.fusengdes.2010.05.004

Google Scholar

[12] S. Zhao, X. Zhou, J. Yu, P. Mummery, SiC/SiC composite fabricated with carbon nanotube interface layer and a novel precursor LPVCS, Fusion Eng. Des. 89 (2014) 131-136.

DOI: 10.1016/j.fusengdes.2014.01.051

Google Scholar

[13] W. Yang, H. Araki, A. Kohyama, Q. Yang, Y. Xu, J. Yu, T. Noda, The effect of SiC nanowires on the flexural properties of CVI-SiC/SiC composites, J. Nucl. Mater. 367-370 (2007) 708-712.

DOI: 10.1016/j.jnucmat.2007.03.092

Google Scholar

[14] W. Yang, H. Araki, A. Kohyama, S. Thaveethavorn, H. Suzuki,T. Noda, Process and Mechanical Properties of in Situ Silicon Carbide-Nanowire-Reinforced Chemical Vapor Infiltrated Silicon Carbide/Silicon Carbide Composite, J. Am. Ceram. Soc. 87 (2004).

DOI: 10.1111/j.1551-2916.2004.01720.x

Google Scholar

[15] W. Yang, H. Arakia, A. Kohyamab, S. Thaveethavorna, H. Suzukia, T. Nodaa, Fabrication in-situ SiC nanowires/SiC matrix composite by chemical vapour infiltration process, Mater. Lett. 58 (2004) 3145-3148.

DOI: 10.1016/j.matlet.2004.05.059

Google Scholar

[16] W. Yang, H. Araki, A. Kohyama, Y. Katoh, Q. Hu, H. Suzuki, T. Noda. Tyranno-SA/SiC composite with SiC nanowires in the matrix by CVI process, J. Nucl. Mater. 329-333 (2004) 539-543.

DOI: 10.1016/j.jnucmat.2004.04.113

Google Scholar

[17] W.J. Kim, S.M. Kang, J.Y. Park, W.S. Ryu, Effect of a SiC whisker formation on the densification of Tyranno SA/SiC composites fabricated by the CVI process, Fusion Eng. Des. 81 [8-14] (2006) 931-936.

DOI: 10.1016/j.fusengdes.2005.07.013

Google Scholar

[18] S. Zhao, Z. Yang, X. Zhou, Microstructure and mechanical properties of compact SiC/SiC composite fabricated with an infiltrative liquid precursor, J. Am. Ceram. Soc. 98.

DOI: 10.1111/jace.13451

Google Scholar

[4] (2015)1332–1337.

Google Scholar

[19] G. Li, X. Li, H. Wang, L. Liu, Ultra long SiC nanowires with fluctuating diameters synthesized in a polymer pyrolysis CVD route, Solid State Sci. 11 (2009) 2167-2172.

DOI: 10.1016/j.solidstatesciences.2009.09.003

Google Scholar

[20] P.D. Yang, C.M. Lieber, Nanorod-superconductor composites: a pathway to materials with high critical current densities, Science 273 (1996) 1791-1794.

DOI: 10.1126/science.273.5283.1836

Google Scholar

[21] R.S. Wagner, W. C Ellis, Vapor-liquid-solid mechanism of single crystal growth, Appl. Phys. Lett. 4.

Google Scholar

[5] (1964) 89-91.

Google Scholar

[22] K.L. Wallis, M. Wieligor, T.W. Zerda, S. Stelmakh, S. Gierlotka, B. Palosz, Stacking fautlts in SiC nanowires, J. Nanosci. Nanotechno. 8.

DOI: 10.1166/jnn.2008.163

Google Scholar

[7] (2008) 3504-3510.

Google Scholar