Crystallisation of Amorphous Al60Fe20Ti15Ni5 Alloy Produced by Mechanical Alloying

Marek Krasnowski; Tadeusz Kulik

doi:10.4028/www.scientific.net/SSP.163.243

Paper Titles

Crystallization and Optimization of Soft Magnetic Properties Effect in FeSiB, FeNbSiB, FeCuNbSiB, FeCuZrCoSiB Amorphous Alloys
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Magnetic and Electric Properties of FeNbB Melt Spun Ribbons
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Preparation of Fe-Based Bulk Amorphous and Nanocrystalline Alloys by Mould Suction Casting Technique
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The X-Ray Studies on Amorphous Fe₇₈Nb₂B₂₀ Alloy
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Crystallisation of Amorphous Al₆₀Fe₂₀Ti₁₅Ni₅ Alloy Produced by Mechanical Alloying
p.243

Thermal Expansibility of 310S Steel-Based PVD Coating in Presence of Metastable Phase
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High Temperature Study of Metamict Steenstrupine
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XRD Multi-Temperatures Study of N,N'-bis(2-Hydroxyethyl)Benzene-1,4-Dicarboxamide
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X-Ray Topography Study of the Nickel Superalloy CMSX-4 Single Crystals
p.260

HomeSolid State PhenomenaSolid State Phenomena Vol. 163Crystallisation of Amorphous Al60Fe20Ti15Ni5 Alloy...

Crystallisation of Amorphous Al₆₀Fe₂₀Ti₁₅Ni₅ Alloy Produced by Mechanical Alloying

Abstract:

In the present work, an elemental powder mixture of Al60Fe20Ti15Ni5 (at.%) was mechanically alloyed in a high-energy ball mill. The phase transformations occurring in the material during milling were studied with the use of X-ray diffraction. The results obtained show that an amorphous phase was formed during performed mechanical alloying process. Thermal behaviour of the milling product was examined by differential scanning calorimetry. It was found that amorphous phase crystallised above 540 °C when a heating rate of 40 °C/min was applied. On the basis of X-ray diffraction results, crystallisation product was identified as a cubic phase with the lattice parameter a0 = 11.856 Å, isomorphic with the 2 (Al2FeTi, fcc structure D8a) phase. The mean crystallite size of the crystallised 2 phase was 19 nm.