Structural Reinvestigation of Alkali Hexatitanate

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Na1.614Li0.386Ti6O13 Single crystal was synthesized by a Li+ ion-exchange method from Na2Ti6O13 single crystal in a molten salt of LiNO3. The obtained Na1.614Li0.386Ti6O13 single-crystal is colorless and has the shape of a rod. Na1.614Li0.386Ti6O13 crystallizes in the monoclinic tunnel type structure, space group C2/m, and lattice parameters a = 15.144(2) Å, b = 3.7492(5) Å, c = 9.162(2) Å and β = 99.0131(9)º. The structure was determined by a single-crystal X-ray study and refined to the conventional values of R = 0.0247 and wR = 0.0451 for 969 independent observed reflections.

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Periodical:

Solid State Phenomena (Volume 170)

Edited by:

J.-L. Bobet, B. Chevalier and D. Fruchart

Pages:

208-212

DOI:

10.4028/www.scientific.net/SSP.170.208

Citation:

K. Kataoka et al., "Structural Reinvestigation of Alkali Hexatitanate", Solid State Phenomena, Vol. 170, pp. 208-212, 2011

Online since:

April 2011

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$35.00

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