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Effect of Surface Treatment of Titanium Elements on the Bond Strength to Zirconium Dioxide

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Abstract:

The aim of the study was to examine the effect of surface treatment of titanium elements on the bond strength to zirconium dioxide. Forty cylindrical titanium discs (Tritan CpTi 1) were divided into four groups (n=10) that were subject to: grinding (Group A), grinding and acid-etching with 5% HF (Group B), sandblasting with 60μm alumina particles (Group C) and sandblasting with 60μm alumina particles and acid-etching with 5% HF (Group D). Prepared materials were bonded to cylindrical discs made of zirconium dioxide (Ceramill Zi) by composite cement (Panavia F 2.0). The specimens were tested for the shear bond strength. The load was applied to the moment of the bond failure. Than the debonded specimens were vertically sectioned and the fractographic analysis of interfacial fractures under SEM as well as the analysis of chemical composition of the obtained fractures using radiographic spectrum were performed. The results were subject to the statistical analysis by using the analysis of variance. The highest values of bond strength were obtained for specimens whose surface was sandblasted and abraded. Fractographic investigation and the analysis of chemical composition of the cross-sections of the interfacial fractures revealed that the fracture occurred at the titanium-resin cement interface. Air abrasion treatment considerably improves the titanium and composite cement bonding and should be recommended for cementation of prosthodontic restorations constructed on titanium implants.

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Periodical:

Solid State Phenomena (Volume 225)

Pages:

151-158

DOI:

https://doi.org/10.4028/www.scientific.net/SSP.225.151

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Online since:

December 2014

Authors:

Beata Śmielak, Marcin Gołębiowski, Leszek Klimek, Emilia Wołowiec*

Keywords:

Shear Bond Strength, Titanium Treatment, Zirconium Dioxide

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© 2015 Trans Tech Publications Ltd. All Rights Reserved

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