The Effect of Heating Rate and Temperature on Mechanical and Microstructure Properties of β-TCP by Microwave Sintering

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This aim of this work was to evaluate the influences of the heating rates and sintering temperatures for sintering β-TCP by microwave furnace. In the first part of work, the heating rates used for sintering β-TCP were including 10, 20, 30 and 40°C/min. Results from physical and mechanical analysis shown that the optimum properties were shown by samples produced at heating rate of 30°C/min. In the second part of the study, the heating rate of 30°C/min was continuing used to sintering samples by different temperatures (1200°C, 1250°C and 1300°C). The sintered sample at 1200°C presented the optimum properties in the physical and mechanical analysis. Finally, the sintered samples by the heating rate 30°C/min at 1200°C were in immersed in SBF to confirm the bioactivity property of β-TCP.

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Solid State Phenomena (Volume 264)

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91-94

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September 2017

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© 2017 Trans Tech Publications Ltd. All Rights Reserved

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[1] Bose, S., et al., Understanding in vivo response and mechanical property variation in MgO, SrO and SiO2 doped β-TCP. Bone, 2011. 48: p.1282–1290.

DOI: 10.1016/j.bone.2011.03.685

Google Scholar

[2] Banerjee, S., et al., Understanding the influence of MgO and SrO binary doping on the mechanical and biological properties of b-TCP ceramics. Acta Biomaterialia, 2010. 6 p.4167–4174.

DOI: 10.1016/j.actbio.2010.05.012

Google Scholar

[3] Swain, S.K., et al., Microstructure, mechanical characteriazation and cell compatibility of β-tricalcium phosphate reinforced with biodegrasable Fe-Mg metal phase. Journal of the mechanical behavior of biomedical materials, 2016. 53: pp.434-444.

DOI: 10.1016/j.jmbbm.2015.09.002

Google Scholar

[4] Dey, A., et al., A comparative study of conventionally sintered, microwave sintered and hot isostatic press sintered NZP and CZP structures interacted with fluoride. Ceramics international, 2013. 39: pp.9531-9359.

DOI: 10.1016/j.ceramint.2013.05.053

Google Scholar

[5] Coovattanachai O, Tosangthum N, Morakotjinda M, Yotkaew T, Krataitong R, Vetayanugul B, Tongsri R. Effect of heating rate on sintered series 300 stainless steel. Songklanakarin J. Sci. Technol 2010; 32 (2): 163-167.

DOI: 10.1016/j.msea.2006.09.105

Google Scholar

[6] Chanda A, Dasgupta S, Bose S, Bandyopadhyay A. Microwave sintering of calcium phosphate ceramics. Materials Science and Engineering 2009; 29: 1144-49.

DOI: 10.1016/j.msec.2008.09.008

Google Scholar

[7] Hung IM, Shih WJ, Hon MH, Wang MC. The Properties of Sintered Calcium Phosphate with [Ca]/[P] = 1. 50 International Journal of Molecular Sciences 2012; 13: 13569-86.

DOI: 10.3390/ijms131013569

Google Scholar

[8] Xin R, Chen J, Zhang Q, . A comparative study of calcium phosphate formation on bioceramics in vitro and in vivo. Biomaterials 2005; 26: 6477–86.

DOI: 10.1016/j.biomaterials.2005.04.028

Google Scholar