Influence of Particle Size and Calcination Temperature on the Abrasiveness of Garnet for Water Jet Cutting of Tough Materials

Article Preview

Abstract:

This study shows the influence of calcinations temperature and particle size of natural garnet mineral on its hardness and abrasiveness (H/A) for use in water jet cutting of tough materials. A standard commercial sample of the mineral was characterized in terms of the hardness and abrasiveness properties. The sample was sized to 4 fractions having the size of <60 um, > 60 < 100 um, > 100 < 200 um and > 200 < 250 um designated the symbols, FF, MF, MC and C respectively. Each fraction was separately heated in controlled conditions at temperatures up to 1000°C at a heating rate of 10°C/min in an electrically heated tube furnace. Soaking time at the maximum temperature was 60 minutes. Hardness and abrasiveness properties of the heat treated samples were tested to cut marble having a thickness of 30 mm. Results revealed that H/A of the garnet mineral increased by heating at temperatures up to 750°C and exhibited gradual decrease with higher temperatures up to 1000°C. Results were explained in the light of a structural irreversible metamorphism (SM) of the garnet crystals; almandine Fe2 + 3Al2Si3O12 and propel Mg3Al2Si3O12. Metamorphism involved reorientation of the crystals followed by coherence to form dense grouping. At higher temperature, irreversible thermal expansion of the structure sets in. Characterization of the mineral was carried out with the help of XRD, SEM and FT-IR measurements.

You might also be interested in these eBooks

Info:

Periodical:

Solid State Phenomena (Volume 277)

Pages:

17-26

Citation:

Online since:

June 2018

Authors:

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2018 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] Xu, Y.N., Ching, W.Y., & Brickeen, B.K. (2000). Electronic structure and bonding in garnet crystals Gd3Sc2Ga3O12, Gd3Sc2Al3O12, and Gd3Ga3O12 compared to Y3Al3O12. Physical Review B, 61(3), 1817-1824.

Google Scholar

[2] Kumar, K. K., Balaram, V., & Sirdeshmukh, L. (1992). Characterization and dielectric properties of almandine-pyrope garnet. Bulletin of Materials Science, 15(3), 279-284.

DOI: 10.1007/bf02927506

Google Scholar

[3] Mao, Z., Lin, J.-F., Huang, S., Chen, J., Xiao, Y., & Chow, P. (2013). Synchrotron Mossbauer study of Fe-bearing pyrope at high pressures and temperatures. American Mineralogist, 98(7), 1146-1152.

DOI: 10.2138/am.2013.4321

Google Scholar

[4] Huggins, F.E. (1975). 3D levels of ferrous-ions in silicate garnets. American Mineralogist, 60(3-4), 316-319.

Google Scholar

[5] Amthauer, G., Annerste, H., & Hafner, S.S. (1976). The Mössbauer spectrum of 57Fe in silicate garnets. Zeitschrift Für Kristallographie – Crystalline Materials, 143(1-6).

DOI: 10.1524/zkri.1976.143.jg.14

Google Scholar

[6] Murad, E. & Wagner, F.E. (1987) The Mössbauer spectrum of almandine. Physics and Chemistry of Minerals, 14, 264-269.

DOI: 10.1007/bf00307992

Google Scholar

[7] Geiger, C.A., Armbruster, T., Lager, G.A., Jiang, K., Lottermoser, W., & Amthauer, G. (1992) A combined temperature dependent Fe Mössbauer and single crystal X-ray diffraction study of synthetic almandine: Evidence for the Gol'danskii Karyagin Effect. Physics and Chemistry of Minerals, 19, 131-126.

DOI: 10.1007/bf00198609

Google Scholar

[8] Cerná, K., Mašlán, M., & Martinec, P. (2000) Mössbauer spectroscopy of garnets a of almandine-propel series. Materials Structure, (7), 6-9.

Google Scholar

[9] K. Barcova, K., Mashlan, M., Zboril, R. Martinec, P. Kula, P. (2000) Thermal decomposition of almandine garnet: Mössbauer study. Czechoslovak Journal of Physics, 51(7), 749-754.

DOI: 10.1023/a:1017618420189

Google Scholar

[10] Zboril, R., Mashlan, M., Machala, L., Walla, J., Barcova, K., & Martinec, P. (2004). Characterization and Thermal Behaviour of Garnets from Almandine-Pyrope Series at 1200°C. ICAME 2003, 403-410.

DOI: 10.1007/978-1-4020-2852-6_61

Google Scholar

[11] Zboril, R., Mashlan, M. , Barcova, K. , Walla, E. Ferrow, J. Martinec P., (2003) Thermal behaviour of propel at 1000 and 1100°C: mechanism of Fe2+ oxidation and decomposition model. Physics and Chemistry of Minerals, 30(10), 620-627.

DOI: 10.1007/s00269-003-0355-x

Google Scholar

[12] Schneeweiss, O., Zbořil, R., David, B., Heřmánek, M., & Mashlan, M. (2009). Solid-state synthesis of α-Fe and iron carbide nanoparticles by thermal treatment of amorphous Fe2O3. ISIAME 2008, 167-173.

DOI: 10.1007/978-3-642-01370-6_21

Google Scholar

[13] Bucher, K., & Frey, M. (2002). Metamorphic Processes. Petrogenesis of Metamorphic Rocks, 49–104.

DOI: 10.1007/978-3-662-04914-3_3

Google Scholar

[14] Whitney, D. L., Lang, H. M., & Ghent, E. D. (1995). Quantitative determination of metamorphic reaction history: mass balance relations between groundmass and mineral inclusion assemblages in metamorphic rocks. Contributions to Mineralogy and Petrology, 120(3-4), 404-411.

DOI: 10.1007/bf00306517

Google Scholar

[15] Touret, J.L. (2001). Fluids in metamorphic rocks. Lithos, 55(1-4), 1-25.

Google Scholar

[16] Novel composite coatings containing (TiC-Al2O3) powder. Materials Science and Engineering: A, 447(1-2), 87–94.

Google Scholar

[17] Novak, G.A., & Gibbs G.V., (1971), Structure of sodium perborate monohydrate crystallography, Am. Mineral, 56, 790-825.

Google Scholar