Investigation of the Tensile Fracture Behavior of Notched C/SiC Composite Using In Situ SEM and Micro-CT

Abstract:

In order to better understand the failure mechanism of C/SiC composites, the tensile behavior of notched C/SiC composites was investigated by the in-situ scanning electron microscopy (SEM) and the micro-CT technique. Surface morphologies of the C/SiC sample during tensile loading were in-situ observed by SEM, while the three-dimensional microscopic images of the C/SiC sample before loading and after failure were obtained by micro-CT. The results showed that no cracks formed in the initial elastic stage corresponding to the linear part of the load-displacement curve. However, corresponding to the following non-linear part of the load-displacement curve, matrix crack initiation, fiber pull-out, crack propagation and deflection appeared consecutively in the notched region of the sample. What’s more, different crack growth paths existed in different directions of the sample during tensile failure. In general, approximately flat fracture formed in the plying direction and serrated or stepped fracture were observed in the needling direction. It indicated that the in-situ observation method combining SEM and micro-CT can obtain the micro-structure images of the material in different states, which is helpful to analyze the fracture failure mechanism of composites.

• Periodical: Solid State Phenomena (Volume 298)
• Pages: 155-160
• DOI: https://doi.org/10.4028/www.scientific.net/SSP.298.155
• Online since: October 2019
• Authors: Bai Hong Jiang*, Yi Yu, Lei Zhang, Shi Zhang Yu, Xiao Jin Gao
• Keywords: C/SiC, In Situ SEM, Micro-CT, Tensile Fracture

References

[1] Ohnabe H, Masaki S, Onozuka M, et al. Potential application of ceramic matrix components[J]. Composites Part A: Applied Science and Manufacturing,1999,30(4):489-496.

DOI: 10.1016/s1359-835x(98)00139-0

[2] Zhang Litong, Cheng Laifei, Xu Yongdong. Progress in research word of new CMC-SiC[J]. Aeronautical Manufacturing Technology,2003,(1):23-32.

[3] Xu Chenghai, Song Leying, Meng Songhe. Investigation of fracture process of a 5D carbon-carbon composites with in-situ SEM technique[J]. Journal of Solid Rocket Technology,2013,36(4):544-548.

[4] Shi Rong, Hu Gengxiang, Li Hejun, et al. Investigation of Tension fracture process of a 1D-C/C with in-situ SEM [J]. PTCA(PART A: PHYSICAL TESTING),1998,34(3):19-21.

[5] Liu Y F ,Tanaka Y. In situ characterization of tensile damage behavior of a plain-woven fiber-reinforced polymer-derived ceramic composite [J]. Materials Letters ,2003,57:1571-1578.

DOI: 10.1016/s0167-577x(02)01034-0

[6] Chen Yu,Sun Ning,Li Hongzhou,et al. Progress and application of the in-situ SEM technique [J]. NEW CHEMICAL MATERIALS,2012,40(2):43-45.

[7] Mei Hui, Cheng Laifei, Zhang Litong, et al. Damage evolution and Micro-structural Characterization of a Cross-woven C/SiC Composite under Tensile Loading [J]. Journal of the Chinese Ceramic Society,2007,35(2):137-143.

[8] Feng Yanjian, Feng Zude, Liu Yongsheng, et al. Micro-CT analysis of high temperature creep damage of 2D C/SiC composites [J]. Heat Treatment of Metals,2011,36:482-485.