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Paper Titles
Preface
A Short History of MIT Studies on Fluid Flow in Solidification, 1952- 2009
Variation of Microstructure and Mechanical Properties of ZW61 Magnesium Alloy Solidified under Different Pressures
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Short-Term Oxidation Behavior, Microstructure Evolution and Compression Behavior of Nickel-Based Superalloy GH4037 in Solid and Semi-Solid States
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Heat-Resistant Al-Alloys with Quasicrystalline and L12- Precipitates
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Using Micro-CT Scanning to Quantitative Characterize Porosity in High Pressure Die Castings and Semi-Solid Castings
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Short-Term Oxidation Behavior, Microstructure Evolution and Compression Behavior of Nickel-Based Superalloy GH4037 in Solid and Semi-Solid States

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Abstract:

Semi-solid processing combines the advantages of traditional forging and casting methods, so it has received much attention recently. However, the research on semi-solid behaviors of Nickel-based superalloys has been rarely reported. In order to investigate the behaviors of Nickel-based superalloy at solid and semi-solid states, oxidation experiments, isothermal treatment experiments and deformation experiments of GH4037 alloy were studied. Short-term oxidation experiments of GH4037 alloy were carried out at a solid temperature (1200 °C) and a semi-solid temperature (1360 °C). The results indicated that the oxides formed at 1200 °C were mainly composed of TiO2, Cr2O3 and a small amount of spinels NiCr2O4, while the oxides formed at 1360 °C consisted of the spinels of NiCr2O4, NiWO4 and NiMoO4 besides TiO2 and Cr2O3. Microstructure evolution of GH4037 alloy after semi-solid isothermal treatment at 1370 °C and 1380 °C was studied. The results indicated that semi-solid microstructures consisted of equiaxed solid grains and liquid phases. The average grains size and shape factor of solid grains were affected by melting mechanism and grain growth mechanism. Compression behaviors of GH4037 alloy after compressed at 1200 °C and 1360 °C were investigated. The results indicated that the flow stress of 1360 °C decreased significantly compared to that of 1200 °C. The deformation zones in the specimens were divided into three parts: the difficult deformation zone, the large deformation zone, and the free deformation zone. At 1200 °C, the deformation mechanism was plastic deformation mechanism. At 1360 °C, sliding between solid particles (SS), liquid flow (LF), flow of liquid incorporating solid particles (FLS), plastic deformation of solid particles (PDS) coexisted in the compression specimen.

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Periodical:

Solid State Phenomena (Volume 327)

Pages:

11-25

DOI:

https://doi.org/10.4028/www.scientific.net/SSP.327.11

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Online since:

January 2022

Authors:

Guan Fei Xiao, Ju Fu Jiang*, Ying Wang, Ying Zhe Liu, Ying Zhang, Min Jie Huang

Keywords:

Deformation Behavior, Microstructure Evolution, Nickel-Based Superalloy, Oxidation Behavior, Semi-Solid Processing

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References

[1] E. Gozlan, M. Bamberger, S.F. Dirnfeld, B. Prinz, J. Klodt, Topologically close-packed precipitations and phase diagrams of NiMoCr and NiMoFe and of NiMoFe with constant additions of chromium, Mater. Sci. Eng. A 141 (1991) 85-95.

DOI: 10.1016/0921-5093(91)90712-v

Google Scholar

[2] X.D. Lu, J.H. Du, Q. Deng, High temperature structure stability of GH4169 superalloy, Mater. Sci. Eng. A 559 (2013) 623-628.

DOI: 10.1016/j.msea.2012.09.001

Google Scholar

[3] T.M. Pollock, Alloy design for aircraft engines, Nat. Mater. 15 (2016) 809-815.

Google Scholar

[4] D. Furrer, H. Fecht, Ni-based superalloys for turbine discs, JOM-US 51 (1999) 14-17.

DOI: 10.1007/s11837-999-0005-y

Google Scholar

[5] T.M. Pollock, S. Tin, Nickel-Based Superalloys for Advanced Turbine Engines: Chemistry, Microstructure and Properties, J. Propul. Power. 22 (2006) 361-374.

DOI: 10.2514/1.18239

Google Scholar

[6] H. Fecht, D. Furrer, Processing of Nickel-Base Superalloys for Turbine Engine Disc Applications, Adv. Eng. Mater. 2 (2010) 777-787.

DOI: 10.1002/1527-2648(200012)2:12<777::aid-adem777>3.0.co;2-r

Google Scholar

[7] X.Z. Lv, F. Sun, J.Y. Tong, Q. Feng, J.X. Zhang, Paired Dislocations and Their Interactions with γ' Particles in Polycrystalline Superalloy GH4037, J. Mater. Eng. Perform. 24 (2015) 143-148.

DOI: 10.1007/s11665-014-1307-y

Google Scholar

[8] F. Sun, J.Y. Tong, Q. Feng, J.X. Zhang, Microstructural evolution and deformation features in gas turbine blades operated in-service, J. Alloys Compd. 618 (2015) 728-733.

DOI: 10.1016/j.jallcom.2014.08.246

Google Scholar

[9] N.K. Park, I.S. Kim, Y.S. Na, J.T. Yeom, Hot forging of a nickel-base superalloy, J. Mate. Process. Technol. 111 (2001) 98-102.

DOI: 10.1016/s0924-0136(01)00489-7

Google Scholar

[10] L. Kunz, P. Lukáš, R. Konečná, S. Fintová, Casting defects and high temperature fatigue life of IN 713LC superalloy, Int J. Fatigue 41 (2012) 47-51.

DOI: 10.1016/j.ijfatigue.2011.12.002

Google Scholar

[11] M.C. Flemings, Behavior of metal alloys in the semisolid state, Metall. Trans. A 22 (1991) 269-293.

Google Scholar

[12] C.P. Wang, Y.Y. Zhang, D.F. Li, H.S. Mei, W. Zhang, J. Liu, Microstructure evolution and mechanical properties of ZK60 magnesium alloy produced by SSTT and RAP route in semi-solid state, Trans. Nonferrous Met. Soc. China 23 (2013) 3621-3628.

DOI: 10.1016/s1003-6326(13)62909-x

Google Scholar

[13] S. Nafisi, O. Lashkari, R. Ghomashchi, F. Ajersch, A. Charette, Microstructure and rheological behavior of grain refined and modified semi-solid A356 Al-Si slurries, Acta Mater. 54 (2006) 3503-3511.

DOI: 10.1016/j.actamat.2006.03.016

Google Scholar

[14] Y.F. Wang, S.D. Zhao, X.Z. Zhao, Y.Q. Zhao, Microstructural coarsening of 6061 aluminum alloy semi-solid billets prepared via recrystallization and partial melting, J. Mech. Sci. Technol. 31 (2017) 3917-3923.

DOI: 10.1007/s12206-017-0737-5

Google Scholar

[15] Q. Q. Zhang, Z.Y. Cao, Y.B. Liu, J.H. Wu, Y.F. Zhang, Study on the microstructure evolution and rheological parameter of semisolid Mg-10Al-4Zn alloys, Mater. Sci. Eng. A 478 (2008) 195-200.

DOI: 10.1016/j.msea.2007.05.095

Google Scholar

[16] W. Liu, D.D. Yang, G.F. Quan, Y.B. Zhang, D.D. Yao, Microstructure Evolution of Semisolid Mg-2Zn-0.5Y Alloy during Isothermal Heat Treatment, Rare Met. Mater. Eng. 45 (2016) 1967-1972.

DOI: 10.1016/s1875-5372(16)30155-2

Google Scholar

[17] B. Amin-Ahmadi, H. Aashuri, Semisolid structure for M2 high speed steel prepared by cooling slope, J. Mate. Process. Technol. 210 (2010) 1632-1635.

DOI: 10.1016/j.jmatprotec.2010.05.011

Google Scholar

[18] T. Balan, E. Becker, L. Langlois, R. Bigot, A new route for semi-solid steel forging, CIRP Ann. Manuf. Technol. 66 (2017) 297-300.

DOI: 10.1016/j.cirp.2017.04.111

Google Scholar

[19] S.J. Park, S.M. Seo, Y.S. Yoo, H.W. Jeong, H.J. Jang, Effects of Al and Ta on the high temperature oxidation of Ni-based superalloys, Corros. Sci. 90 (2015) 305-312.

DOI: 10.1016/j.corsci.2014.10.025

Google Scholar

[20] D. Saber, I.S. Emam, R. Abdel-Karim, High temperature cyclic oxidation of Ni based superalloys at different temperatures in air, J. Alloys Compd. 719 (2017) 133-141.

DOI: 10.1016/j.jallcom.2017.05.130

Google Scholar

[21] L. Qin, Y.L. Pei, S.S. Li, X.B. Zhao, S.K. Gong, H.B. Xu, Role of volatilization of molybdenum oxides during the cyclic oxidation of high-Mo containing Ni-based single crystal superalloys, Corros. Sci. 719 (2017) 133-141.

DOI: 10.1016/j.corsci.2017.08.025

Google Scholar

[22] E.D. Manson-Whitton, I.C. Stone, J.R. Jones, P.S. Grant, B. Cantor, Isothermal grain coarsening of spray formed alloys in the semi-solid state, Acta Mater. 50 (2002) 2517-2535.

DOI: 10.1016/s1359-6454(02)00080-0

Google Scholar

[23] Y.L. Lu, M.Q. Li, W.C. Huang, H.T. Jiang, Deformation behavior and microstructural evolution during the semi-solid compression of Al-4Cu-Mg alloy. Mater. Charact. 54 (2005) 423-430.

DOI: 10.1016/j.matchar.2005.01.013

Google Scholar

[24] B. Liu, X.G. Yuan, H.J. Huang, S.H. Zhang, Semi-Solid Deformation of Al-Fe Alloy Prepared by Electromagnetic Stirring. Adv. Mater. Res. 152 (2011) 726-733.

DOI: 10.4028/www.scientific.net/amr.152-153.726

Google Scholar

[25] J.G. Wang, P. Lu, H.Y. Wang, Q.C. Jiang, Effect of predeformation on the semisolid microstructure of Mg-9Al-0.6Zn alloy, Mater. Lett. 58 (2004) 3852-3856.

DOI: 10.1016/j.matlet.2004.07.044

Google Scholar

[26] Y.Q. Zhao, W.L. Wu, H. Chang, Research on microstructure and mechanical properties of a new α + Ti2Cu alloy after semi-solid deformation, Mater. Sci. Eng. A 416 (2006) 181-186.

DOI: 10.1016/j.msea.2005.10.038

Google Scholar

[27] M. Yi, S. Sugiyama, J. Yanagimoto, Microstructural evolution during RAP process and deformation behavior of semi-solid SKD61 tool steel, J. Mate. Process. Technol. 212 (2012) 1731-1741.

DOI: 10.1016/j.jmatprotec.2012.04.003

Google Scholar

[28] J.F. Jiang, G.F. Xiao, W. Ying, Y.S. Qi, Microstructure evolution of wrought nickel based superalloy GH4037 in the semi-solid state, Mater. Charact. 141 (2018) 229-237.

DOI: 10.1016/j.matchar.2018.04.057

Google Scholar

[29] P.K. Seo, C.G. Kang, The effect of raw material fabrication process on microstructural characteristics in reheating process for semi-solid forming, J. Mate. Process. Technol. 162 (2005) 402-409.

DOI: 10.1016/j.jmatprotec.2005.02.012

Google Scholar

[30] A. Sato, Y.L. Chiu, R.C. Reed, Oxidation of nickel-based single-crystal superalloys for industrial gas turbine applications, Acta Mater. 59 (2011) 225-240.

DOI: 10.1016/j.actamat.2010.09.027

Google Scholar

[31] R. Haugsrud, On the high-temperature oxidation of nickel, Corros. Sci. 45 (2003) 211-235.

Google Scholar

[32] J.D. Cao, J.S. Zhang, R.F. Chen, Y.X. Ye, Y.Q. Hua, High temperature oxidation behavior of Ni-based superalloy GH202, Mater. Charact. 118 (2016) 122-128.

DOI: 10.1016/j.matchar.2016.05.013

Google Scholar

[33] Q.Q. Shi, J. Liu, W. Wang, W. Yan, Y.Y. Shan, K. Yang, High Temperature Oxidation Behavior of SIMP Steel, Oxid. Met. 83 (2015) 521-532.

DOI: 10.1007/s11085-015-9532-9

Google Scholar

[34] D.W. Yun, S.M. Seo, H.W. Jeong, I.S. Kim, Y.S. Yoo, Modelling high temperature oxidation behaviour of Ni-Cr-W-Mo alloys with Bayesian neural network, J. Alloys Compd. 587 (2014) 105-112.

DOI: 10.1016/j.jallcom.2013.10.138

Google Scholar

[35] H. Zhang, Y. Liu, X. Chen, H.W. Zhang, Y.X. Li, Microstructural homogenization and high-temperature cyclic oxidation behavior of a Ni-based superalloy with high-Cr content, J. Alloys Compd. 727 (2017) 410-418.

DOI: 10.1016/j.jallcom.2017.08.137

Google Scholar

[36] S.C. Hardy, P.W. Voorhees, Ostwald ripening in a system with a high volume fraction of coarsening phase, Metall. Trans. A 19 (1988) 2713-2721.

DOI: 10.1007/bf02645806

Google Scholar

[37] J. Wang, H. Xiao, L.B. Wu, H.L. Hu, D.H. Lu, R.F. Zhou, R. Zhou, Deformation characteristic of semi-solid ZCuSnl0 copper alloy during isothermal compression, Rare Met. 35 (2016) 620-626.

DOI: 10.1007/s12598-015-0479-4

Google Scholar

[38] C.P. Chen, C.Y.A. Tsao, Semi-solid deformation of non-dendritic structures-I. Phenomenological behavior, Acta Mater. 45 (1997) 1955-1968.

DOI: 10.1016/s1359-6454(96)00312-6

Google Scholar

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