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Online since: November 2020
Authors: Mária Gabániová
A number of different surface chemistry-based defects are related to annealing process.
An investigation into this defect found the cause of this region of low reflectivity was the formation of surface chromium and manganese spinel oxides (MnCr2O4) along grain boundaries.
When polycrystalline materials are selectively oxidized grain boundaries can act as fast diffusion paths.
So oxide precipitates are commonly observed at the intersections between the grain boundaries at the free surface when low alloy steel is annealed.
The micrographs revealed in one case the incompact tin coating with dark “islands” (Fig. 2a) and significant grain boundaries in compact tin coating on the second one (Fig. 2b).
Online since: August 2020
Authors: Ekaterina Borisovna Markova, Alexander Genrihovich Cherednichenko, V.V. Kurilkin, J.M. Serov
The formation of various defects contributes to the course of the dehydrogenation or degradation reaction due to the different number of catalytic centers.
This method leads to the production of coarse-grained materials having a low specific surface area.
a - Gd2Zr2O7 (I) b - Gd2Zr2O7 (II) Shape of grains, size Hexagonal, size ~ 0.01 mm Isometric, size ~ 0.01 mm Fig 1.
This allowed us to use a comparative method for finding the number of PACs.
Sample Adsorption capacity, mmol/g Number of PACs, mmol/g Mean number of molecules in a cluster Specific adsorptioncapacity, μmol/m2 Gd2Zr2O7(I) 19,7 0,3 65 80 Gd2Zr2O7(II) 15,9 0,2 40 13 Based on this, it can be assumed that depending on the synthesis, differently deformed structures of the same compound are obtained.
Online since: July 2015
Authors: Jian Li Yang, Mei Li Du, Tian Qin Zang
Introduction Fly ash is a fine-grained and dispersed remnants after coal or pulverized coal combustion, it is a main solid waste discharged from coal-fired power plants.
(2) XRD analysis Strong diffraction peaks can be seen only in the 20-30 diffraction angle region from figure 1, while the number of diffraction peaks is little in the other angles and the intensity is very small, almost do not see the formation of 4A molecular sieve.
This indicates that large numbers of vitreous exit which does not transform, crystallinity degree of product is low.
The figure shows, the number of product peaks is numerous, the intensity of diffraction peaks is strong, consistent with the standard map data of 4A molecular sieve.
(3) SEM observation Shown in Figure 4, after adding 8% directing agent, the shape of the synthetic products is regular, crystals are uniform, profile is clear, purity is high, while the grain size reduced and synthesis effect is better.
Online since: April 2024
Authors: Anatoliy Samelyuk, Oksana Kornienko, Andrey Ragulya, Maryna Zamula, Valeriy Kolesnichenko, Yuriy Yurchenko, Oleksandr Shyrokov, Tamara Tomila, Andriy Kotko
Despite the rather high density of the obtained sample (99.7%), it remains translucent for a number of reasons: the obtained sample is characterized by randomly oriented grains, which creates additional optical scattering.
In case of further elevation of the heat treatment temperature of the starting material, an increase in grain size will be observed, which is undesirable when creating a dense material.
The reason for the insufficiently high transparency may be: variable refraction in anisotropic media and a wide grain size distribution in the resulting ceramics.
Despite the rather high density of the obtained sample (99.7%), it remains translucent for a number of reasons: the obtained sample is characterized by randomly oriented grains, which creates additional optical scattering.
Obtaining transparent polycrystalline ceramics with a non-cubic structure requires precise control of grain orientation so that optical scattering losses are minimized.
Online since: June 2009
Authors: Zhi Min Yin, Guo Ping Xu, Gen Xu, Rong Chao Jiang
One is the so-called microstress which usually exists within one or among several grains, and when it is released there is no macrostrain.
A plot of detected number of photons versus Raman shift from the incident laser energy gives a Raman spectrum.
The average size of diamond grains of PDC is 25µm.
The test of the diamond grains and that of the PDC was conducted in the same condition and on the same apparatus to eliminate the systematic errors.The grains were tested three times and the wavenumbers are 1331.77cm -1.
Wavenumbers of the diamond powders in grain size 28µm and 5µm that are used as raw materials in the synthesis of PDC were also measured.
Online since: August 2015
Authors: Mourad Khelifa, Van Diem Thi
Timber exhibits its greatest strength parallel to the grain; development of end joints that can transmit a significant proportion of this strength has been the main objective of many research works carried out in this field recently [1-3].
The problem is that timber cannot be jointed sufficiently well, end grain to end grain with existing cohesive and methods to be of any practical signification.
However, timber can be bonded easily quite effectively with most adhesives side grain to side grain.
LVDT Grain orientation 300 F F 300 252 932 42 80 (b).
Nevertheless, the effect of the different length and the number of CFRP layers of finger-jointed timber beams still need to be considered in further work.
Online since: May 2011
Authors: Xiao Yong Li, Kang Xu, Si Yuan Wang
Carried on the conventional experiment in lab with the fine grain, including proportion experiment, heavy compaction test, fluid plastic limit test, grading analysis test, direct shearl test, compressive test.
The test result of fine grain soil is seen in Table 1.
The test result of coarse grained soil is seen in Table 2.
type Ground coefficient(MPa/m) K30 K35 k40 k45 k50 k55 k60 k65 k70 k75 Fine-grain soil 90.45 80.95 74.36 62.41 56.57 50.76 46.18 42.98 41.80 41.70 Aggregate 113.61 100.41 90.91 78.95 69.15 63.35 60.27 53.61 50.94 49.40 Aggregate Fine-grain R2=0,995 Ground coefficient (MPa/m) R2=0,997 Fig. 5 Ground coefficient versus diemeter of load plate It can be seen that the ground coefficient and the load plate diameter existence good misalignment relevance from Figure 5.
The regression equation for fine grain soil is (1) Where k is ground coefficient and D is load plate diameter.
Online since: October 2006
Authors: H. Lee, Y. Pontikes, G.N. Angelopoulus, Ungsoo Kim, William Carty
Under a more stringent legislative demand for environmental and social sustainability, efforts are intensified for the reuse of the material in other industrial processes and a number or BR-derived products is available in the market [3].
Mixture S3 is similar to S1 but in this case coarse grained quartz has been used instead of flint.
Best results are obtained for mixture W, the mixtures with polymers addition, S3, and S5, and the one with coarse grained quartz S3.
Best results are obtained for mixture W, the mixtures with polymers addition, S4 and S5, and the one with coarse grained quartz S3.
In mixture S3, the addition of coarse-grained quartz had as a result slightly reduced maximum cohesion compared to S1.
Online since: June 2011
Authors: Guo Xin Hu, Liang Liang Liu, Feng Gao, Xiao Cao
The abnormally large grains may be attributed to sintering in the presence of the liquid phase.
This may be due to the effect of the low melting point of Al2O3-MgO on the grain growth behavior of the ceramics.
This low melting point additive diffuses into the grain boundary, allowing BSTO grains to grow rapidly with a cubic shape corresponding to their crystal structure.
When the content of Al2O3 is increased up to 20wt%, the number of abnormal grains increases and more pores appear, which is consistent with the density date of the samples shown in Part 2.
With the increase of Al2O3 content, the grains sizes of ceramics become larger.
Online since: January 2017
Authors: Chun Hua Ma, Zhi Wen Lu, Tie Ye
The precipitation of Nb has the effect of precipitation hardening and grain refinement.
After deforming in the recrystallization range, the larger or non-recrystallized austenite grains were quickly refined whereas smaller austenite grains were slowly refined.
The strengthening mechanisms are chiefly grains refining and solution reinforcing.
Most of precipitates are dissolved in ferrite, and a large number of fine V (C.
The grain size gets smaller and its strength increases markedly duo to the small grain size, dispersion strengthening and working hardening.
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