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Online since: February 2007
Authors: Hua Nan Wang, Hong Li, Yuan Hua Mu, Yu Bao Li, Xue Jiang Wang, Hong Zhao Xiang
Preparation and Characterization of n-HA/PA66/CS Biocomposite
Hongzhao Xiang1,2,a , Yubao Li1,b *, Yuanhua Mu1,2 , Xuejiang Wang
1
,
Huanan Wang1 , Hong Li1,2
1
Research Center for Nano-Biomaterials, Analytical & Testing Center, Sichuan University
2
College of Chemistry, Sichuan University, Chengdu, P.
As we know, chitosan has different structure in the different acid solution.
When acetic acid is used as solvent, the chitosan shows structure of TypeⅡ(the extended eight-fold helical structure with 40.8 Å axial repeat), which is benefit to chalet with metal ion[5].
But the TypeⅡstructure of chitosan was easy to collapse by heat treatment at high temperature, this collapsed structure hindered n-HA to enter into interior of chitosan.
So we think that the crystal of n-HA has a structure and crystal size similar to natural bone.
As we know, chitosan has different structure in the different acid solution.
When acetic acid is used as solvent, the chitosan shows structure of TypeⅡ(the extended eight-fold helical structure with 40.8 Å axial repeat), which is benefit to chalet with metal ion[5].
But the TypeⅡstructure of chitosan was easy to collapse by heat treatment at high temperature, this collapsed structure hindered n-HA to enter into interior of chitosan.
So we think that the crystal of n-HA has a structure and crystal size similar to natural bone.
Online since: November 2011
Authors: Wei Min Zhang, Jia Ling Pu, Yu Lei Zhao, Ji Lei Li, Fan Fan Yu
The structure of the intermediates, monomers and polymers were characterized with FTIR and 1HNMR measurement.
Compared with photoisomerization and photodegradation, photodimerization has more stable chemistry properties and bigger potential applications [3].
All the structures were confirmed by FT-IR and 1H-NMR spectroscopy.
Compared with photoisomerization and photodegradation, photodimerization has more stable chemistry properties and bigger potential applications [3].
All the structures were confirmed by FT-IR and 1H-NMR spectroscopy.
Online since: March 2013
Authors: Zhen Kun Huang, Y. Jiang, Lan Er Wu
Several kinds of structure defects for LPSed SiC were emphasized to discuss.
Some impurities vaporized and formed hole around by a halo (dark), which would affect the neighboring structure (Figure 4(e)).The defect in Figure 4 (f) is due to milling ununiformity of powder mixture of SiC and aid: it could cause the liquid ununiform gathering.
Some metal impurity, like Fe, is incompatible with components of SiC ceramic in physic- chemistry property.
Some impurities vaporized and formed hole around by a halo (dark), which would affect the neighboring structure (Figure 4(e)).The defect in Figure 4 (f) is due to milling ununiformity of powder mixture of SiC and aid: it could cause the liquid ununiform gathering.
Some metal impurity, like Fe, is incompatible with components of SiC ceramic in physic- chemistry property.
Online since: September 2020
Authors: Andrey V. Nomoev, Yuri Ya Gafner, Svetlana L. Gafner
Moreover, the analysis of the external view and the structure of Cu-Au nanoparticles of various chemical composition allowed us to conclude that a large number of binary nanoparticles were of an icosahedral structure.
The structure of particles with D = 2.0-20.0 nm was determined as fcc.
In the end, we can say that in all the experiments carried out, the most diverse structure of Cu-Au nanoparticles was observed without a clear understanding of exactly which structure and shape can be formed as a result of a particular synthesis method.
In addition, the analysis of the external view and the structure of Cu-Au nanoparticles of various chemical composition showed the following peculiar features: a big amount of binary nanoparticles had a pronounced icosahedral structure (Fig. 2).
Alloyeau, New insights into the mixing of gold and copper in a nanoparticle from a structural study of Au-Cu nanoalloys synthesized via a wet chemistry method and pulsed laser deposition, Phys.
The structure of particles with D = 2.0-20.0 nm was determined as fcc.
In the end, we can say that in all the experiments carried out, the most diverse structure of Cu-Au nanoparticles was observed without a clear understanding of exactly which structure and shape can be formed as a result of a particular synthesis method.
In addition, the analysis of the external view and the structure of Cu-Au nanoparticles of various chemical composition showed the following peculiar features: a big amount of binary nanoparticles had a pronounced icosahedral structure (Fig. 2).
Alloyeau, New insights into the mixing of gold and copper in a nanoparticle from a structural study of Au-Cu nanoalloys synthesized via a wet chemistry method and pulsed laser deposition, Phys.
Online since: August 2016
Authors: Sha Ren, Li Na Guo
Hydrothermal Synthesis and Luminescent Properties of
BiPO4:Eu3+ Phosphors
Sha Ren1,a*, Lina Guo1,b
1College of Chemistry and Environmental Science, Inner Mongolia Normal University,
Hohhot 010022, China
asr@imnu.edu.cn, b775735220@qq.com
Keywords: BiPO4: Eu 3+, Luminescent properties, Hydrothermal method.
The structure and composition of the samples were characterized by IR and XRD.
The results showed that with the increase of hydrothermal temperature and hydrothermal time, the crystal structure of BiPO4 changed from hexagonal phase to monoclinic phase.
Different crystal structures of Eu3+ doped BiPO4 samples had the same emission peaks in emission spectra excited by blue light wavelength of 395nm.
The crystal structure changed from hexagonal phase to monoclinic phase when the hydrothermal time was increased from 2h to 10h at the temperature of 160ºC.
The structure and composition of the samples were characterized by IR and XRD.
The results showed that with the increase of hydrothermal temperature and hydrothermal time, the crystal structure of BiPO4 changed from hexagonal phase to monoclinic phase.
Different crystal structures of Eu3+ doped BiPO4 samples had the same emission peaks in emission spectra excited by blue light wavelength of 395nm.
The crystal structure changed from hexagonal phase to monoclinic phase when the hydrothermal time was increased from 2h to 10h at the temperature of 160ºC.
Online since: April 2014
Authors: Chii Ruey Lin, Da Hua Wei, Minh Khoa Bendao
The effects of nitrogen doping level on the structure, optical, and electrical of the as-grown NCD:N was discussed.
The results showed that the micro structure, surface roughness, electrical properties, and optical properties were affected by the nitrogen doping.
In order to obtained Ohmic contact of Al/Si/NCD/Au multilayer structure, annealing procedures were carried out at 450 oC in Ar ambient.
Raman spectra for the NCD films grown in H2-4% CH4 chemistries with addition of N2 concentration ranged from 0% to 20%.
The as-prepared intrinsic diamond film possesses characteristic peaks of NCD includes 1140 cm-1 of C-H bond (polyacetylene, trans- structure), 1332 cm-1 of diamond phase carbon, 1350 and 1580 cm-1 of D and G band of sp2-structure carbon, respectively.
The results showed that the micro structure, surface roughness, electrical properties, and optical properties were affected by the nitrogen doping.
In order to obtained Ohmic contact of Al/Si/NCD/Au multilayer structure, annealing procedures were carried out at 450 oC in Ar ambient.
Raman spectra for the NCD films grown in H2-4% CH4 chemistries with addition of N2 concentration ranged from 0% to 20%.
The as-prepared intrinsic diamond film possesses characteristic peaks of NCD includes 1140 cm-1 of C-H bond (polyacetylene, trans- structure), 1332 cm-1 of diamond phase carbon, 1350 and 1580 cm-1 of D and G band of sp2-structure carbon, respectively.
Online since: October 2012
Authors: Zhi Jun Guo, Wein Feng Chang, Hong Zhu, Wein Duo Yang
It has a tetragonal structure at room temperature and shows a cubic structure above the curie temperature.
The crystal phase and the structure of the PBT thin films were identified by using the X-ray diffraction method.
At x=0.2, the SEM micrograph showed the grain uniformly distributed and the small pore structure appeared in the surface.
However, two phase structures appeared.
Generally, the absorbing radiant energy properties of the molecular were due to the molecular structure.
The crystal phase and the structure of the PBT thin films were identified by using the X-ray diffraction method.
At x=0.2, the SEM micrograph showed the grain uniformly distributed and the small pore structure appeared in the surface.
However, two phase structures appeared.
Generally, the absorbing radiant energy properties of the molecular were due to the molecular structure.
Online since: October 2014
Authors: Chun Yan Lai, Jiao Jiao Wei, Zhen Wang
XRD, SEM and galvanostatic charge/discharge tests were used to analysis the structure and electrochemical performance of Li3V2(PO4)3 materials.
The Li3V2(PO4)3 cathode materials synthesized at 700˚C, 750˚C, 800˚C, 850˚C all have a standard crystal structure.
Physical and Chemistry.
The Li3V2(PO4)3 cathode materials synthesized at 700˚C, 750˚C, 800˚C, 850˚C all have a standard crystal structure.
Physical and Chemistry.
Online since: November 2010
Authors: Gui Yang Liu, Jun Ming Guo, Yan Nan Li, Bao Sen Wang
LiMn2O4 powders prepared by solution combustion synthesis in ethanol and water systems
LIU Gui-yang1, a, GUO Jun-ming2, b, LI Yan-nan3, c, WANG Bao-sen1, d
1College of science, Honghe University, Mengzi, Yunnan, 661100, China
2School of Chemistry and Biotechnology, Yunnan University of Nationalities, Kunming 650031, China
3Library of Honghe University, Mengzi, Yunnan, 661100, China
aliuguiyang@tsinghua.org.cn, bguojunming@tsinghua.org.cn, cliyannan1982@126.com, dwangbs9561@126.com
Keywords: solution combustion synthesis, spinel LiMn2O4, lithium-ion batteries
Abstract.
The structure and morphology of the products have been analyzed by X-ray diffraction (XRD) and scanning electron microscopy (SEM), respectively.
The phases and structures of products were analyzed by XRD (D/max-rB, Japan, Cu-Kα, λ=1.5406Å) in the range of 10 to 70°.
The structure and morphology of the products have been analyzed by X-ray diffraction (XRD) and scanning electron microscopy (SEM), respectively.
The phases and structures of products were analyzed by XRD (D/max-rB, Japan, Cu-Kα, λ=1.5406Å) in the range of 10 to 70°.