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Online since: July 2022
Authors: Rodolfo Fernandez-Martinez, M. Belén Gomez-Mancebo, Laura J. Bonales, Cesar Maffiotte, Alberto J. Quejido, Isabel Rucandio
After graphite oxidation and exfoliation to produce graphene oxide (GO) the reduction of GO is performed to restore or simulating the pristine graphene structure.
Zettl, Determination of the Local Chemical Structure of Graphene Oxide and Reduced Graphene Oxide, Advanced Materials 22 (40) (2010) 4467-4472
TascóN, Vitamin C Is an Ideal Substitute for Hydrazine in the Reduction of Graphene Oxide Suspensions, Journal of Physical Chemistry C - J PHYS CHEM C 114 ((2010) 6426-6432
Nagase, Hydrazine and Thermal Reduction of Graphene Oxide: Reaction Mechanisms, Product Structures, and Reaction Design, The Journal of Physical Chemistry C 114 (2) (2010) 832-842
Mercedes Velazquez, Evolution of the Raman Spectrum with the Chemical Composition of Graphene Oxide, Journal of Physical Chemistry C 121 (37) (2017) 20489-20497
Zettl, Determination of the Local Chemical Structure of Graphene Oxide and Reduced Graphene Oxide, Advanced Materials 22 (40) (2010) 4467-4472
TascóN, Vitamin C Is an Ideal Substitute for Hydrazine in the Reduction of Graphene Oxide Suspensions, Journal of Physical Chemistry C - J PHYS CHEM C 114 ((2010) 6426-6432
Nagase, Hydrazine and Thermal Reduction of Graphene Oxide: Reaction Mechanisms, Product Structures, and Reaction Design, The Journal of Physical Chemistry C 114 (2) (2010) 832-842
Mercedes Velazquez, Evolution of the Raman Spectrum with the Chemical Composition of Graphene Oxide, Journal of Physical Chemistry C 121 (37) (2017) 20489-20497
Online since: August 2019
Authors: Arsen Kharaev, Vadim A. Kvashin, Rima Bazheva, Aleksander N. Kalinnikov, B.Z. Beshtoev, A.S. Borodulin
As the result, PEK had the following structure:
OK and bisphenol A were taken in equimolar amounts.
The results of turbidimetric titration confirmed the structure of polyethers.
From [10], it is known that lower dielectric characteristics correspond to more densely packed polymer structures.
Polyetherketones: synthesis, structure, properties, application (review).
Synthesis and Properties of Halogens Containing Simple and Complex Block Copolyethers //Chemistry and Chemical Technology, 2017, Vol.11, № 2, pp. 162-170
The results of turbidimetric titration confirmed the structure of polyethers.
From [10], it is known that lower dielectric characteristics correspond to more densely packed polymer structures.
Polyetherketones: synthesis, structure, properties, application (review).
Synthesis and Properties of Halogens Containing Simple and Complex Block Copolyethers //Chemistry and Chemical Technology, 2017, Vol.11, № 2, pp. 162-170
Online since: June 2012
Authors: Zulkhair A. Mansurov, Seitkhan Azat, Almagul R. Kerimkulova, Murat K. Gilmanov, Sergazy M. Аdekenov, Bibigul B. Rachimova, S.A. Ibragimova
Results and discussion
The most important information about the structure of the carbonized carbon material can provide scanning electron microscopy.
On this one of the objectives of the study was to develop a method of obtaining highly active bio-stimulator based on the application we have developed a carbon adsorbent with a nanoporous structure.
To do this, drew attention to the work performed in the laboratory of the structure and regulation of the enzymes of the Institute of Molecular Biology and Biochemistry, named after M.A Aitkhozhina.
This experiment was conducted with the assistance of a professor Z.A.Mansurov at the Institute of Biomedical Chemistry V.N.Orehovicha Russian Academy of Medical Sciences.The results of mass spectrometry are presented in Fig. 5.
These results indicate the suitability of the nanoporous structure of the carbon sorbent for the molecular-sieve chromatography of large protein-lipid complexes, such as sferosomy.
On this one of the objectives of the study was to develop a method of obtaining highly active bio-stimulator based on the application we have developed a carbon adsorbent with a nanoporous structure.
To do this, drew attention to the work performed in the laboratory of the structure and regulation of the enzymes of the Institute of Molecular Biology and Biochemistry, named after M.A Aitkhozhina.
This experiment was conducted with the assistance of a professor Z.A.Mansurov at the Institute of Biomedical Chemistry V.N.Orehovicha Russian Academy of Medical Sciences.The results of mass spectrometry are presented in Fig. 5.
These results indicate the suitability of the nanoporous structure of the carbon sorbent for the molecular-sieve chromatography of large protein-lipid complexes, such as sferosomy.
Online since: June 2015
Authors: Zbigniew Grzesik, Stanisław Mrowec, Grzegorz Smola
The Interpretation of Marker Experiment Conducted During Formation of Higher Oxide on the Surface of Lower Oxide
Zbigniew Grzesika, Grzegorz Smolab, Stanislaw Mrowecc
AGH University of Science and Technology, Faculty of Materials Science and Ceramics, Department of Physical Chemistry and Modelling, 30-059 Krakow, A.
The marker method in studying the formation mechanism and defect structure of higher oxide during oxidation of lower oxide has been discussed.
Kröger: The chemistry of Imperfect Crystals (North-Holland Publ.
The marker method in studying the formation mechanism and defect structure of higher oxide during oxidation of lower oxide has been discussed.
Kröger: The chemistry of Imperfect Crystals (North-Holland Publ.
Online since: July 2012
Authors: Lian Jin Weng, Di Geng, Yuan Yuan Han, Xin Yang
METHODS: Compounds were isolated and purified by carious chromatographic techniques and their structures were elucidated by physicochemical and spectral data.
The voucher specimen (collection No. 07-1005) was deposited in the Department of Natural Medicinal Chemistry, China Pharmaceutical University. 2.3 Extraction and Isolation The air-dried whole plant (3.5kg) was finely powdered and extracted with 95% EtOH at 60℃.
Vol 5(1983), p. 1544 [9] Xin’an Wu, Yimin Zhao: China Journal of Chinese Materia Medica Vol. 6(2005), p. 443 [10] Jun Zhao, Ming Lin, Yi Huang, Tao Liu, Yu Zhao: Chinese Pharmaceutical Jour- nal Vol.19(2008), p. 1461 [11] Francesco Mazzini, Emanuele Alpi, Piero Salvadori, Thomas Netscher: European Journal of Organic Chemistry Vol. 7(2003), p. 2840 [12] Nawwar M A M, Buddrus J, Bauer H: Phytochemistry Vol 7(1982), p. 1755 [13] Junwei Zhang: China Journal of Chinese Materia Medica Vol. 1(1989), p. 36 [14] Chunfeng Xie, Zijing Li, Jianbo Qu, Bin Sun and Hong xiang Lou: Chinese Pharmaceutical Journal Vol 22(2007), p. 1706 [15] Paulo J C Benevides, Patrícia Sartorelli and Massuo J Kato: Phytochemistry Vol. 2(1999), p, 339
The voucher specimen (collection No. 07-1005) was deposited in the Department of Natural Medicinal Chemistry, China Pharmaceutical University. 2.3 Extraction and Isolation The air-dried whole plant (3.5kg) was finely powdered and extracted with 95% EtOH at 60℃.
Vol 5(1983), p. 1544 [9] Xin’an Wu, Yimin Zhao: China Journal of Chinese Materia Medica Vol. 6(2005), p. 443 [10] Jun Zhao, Ming Lin, Yi Huang, Tao Liu, Yu Zhao: Chinese Pharmaceutical Jour- nal Vol.19(2008), p. 1461 [11] Francesco Mazzini, Emanuele Alpi, Piero Salvadori, Thomas Netscher: European Journal of Organic Chemistry Vol. 7(2003), p. 2840 [12] Nawwar M A M, Buddrus J, Bauer H: Phytochemistry Vol 7(1982), p. 1755 [13] Junwei Zhang: China Journal of Chinese Materia Medica Vol. 1(1989), p. 36 [14] Chunfeng Xie, Zijing Li, Jianbo Qu, Bin Sun and Hong xiang Lou: Chinese Pharmaceutical Journal Vol 22(2007), p. 1706 [15] Paulo J C Benevides, Patrícia Sartorelli and Massuo J Kato: Phytochemistry Vol. 2(1999), p, 339
Online since: January 2007
Authors: Mi Jeong Han, Ji Young Mang, Dong Hoon Choi
Nitrile-butadiene
rubber (NBR)/OMMT nanocomposites could be obtained using melt-compounding followed by
hot-press vulcanization. d-Spacings of OMMT were changed as the chemical structures of
modifiers were varied.
X-ray diffraction (XRD) and tensile measurements of NBR nanocomposites revealed that the structures of organic modifiers affect the properties of NBR nanocomposites after vulcanization.
The effects of the chemical structures of organic modifiers on interaction between NBR and OMMT, and the properties of NBR/OMMT were evaluated.
The chemical structures of organic modifiers were confirmed 1H and 13 C NMR spectroscopy.
Tensile strengths of NBR/OMMT nanocomposites were dramatically changed by the structures of organic modifies.
X-ray diffraction (XRD) and tensile measurements of NBR nanocomposites revealed that the structures of organic modifiers affect the properties of NBR nanocomposites after vulcanization.
The effects of the chemical structures of organic modifiers on interaction between NBR and OMMT, and the properties of NBR/OMMT were evaluated.
The chemical structures of organic modifiers were confirmed 1H and 13 C NMR spectroscopy.
Tensile strengths of NBR/OMMT nanocomposites were dramatically changed by the structures of organic modifies.
Online since: June 2010
Authors: Efstathios K. Polychroniadis, Mikael Syväjärvi, Rositza Yakimova, Alkyoni Mantzari, Milena Beshkova, Maya Marinova
Polychroniadis1,f
1
Physics Department, Aristotle University of Thessaloniki 54124, Thessaloniki, Greece
2
Department of Physics, Chemistry and Biology, Linköping University, SE-58183 Linköping,
Sweden
a
marinova@physics.auth.gr, bam@auth.gr, cmilbe@ifm.liu.se, dmisyv@ifm.liu.se, eroy@ifm.liu.se,
f
polychr@auth.gr
Keywords: 3C-SiC, 6H-SiC, sublimation epitaxy, TEM, polytypic transformations.
In the present work Conventional and High Resolution Transmission Electron Microscopy has been used to examine the structure and types of interfaces between 3C-SiC and 6HSiC for samples grown by Sublimation Epitaxy.
The growth of bulk ingots and epilayers of quality allowing implementation of devices is not accomplished for the 3C-SiC which crystallizes in the cubic zinc blende structure and has to be grown on 6H-SiC due to the lack of 3C-SiC substrates.
In the present work Conventional and High Resolution Transmission Electron Microscopy has been used to examine the structure and types of interfaces between 3C-SiC and 6HSiC for samples grown by Sublimation Epitaxy.
The growth of bulk ingots and epilayers of quality allowing implementation of devices is not accomplished for the 3C-SiC which crystallizes in the cubic zinc blende structure and has to be grown on 6H-SiC due to the lack of 3C-SiC substrates.
Online since: March 2011
Authors: Dong Jiang, Xiao Ran Zhang, Cheng You Ma, Yan Mei Ma
It was found that the interfacial adhesion was enhanced, the size of the dispersed phase was reduced and PES and PC formed an interlocking structure with the copolymer, which suggest the addition of the compatibizer may improved the miscibility between PES and PC, and result in the improvement of the mechanical properties of the blends.
Materials: PES was obtained from the chemistry department of Jilin University.
Thomason*, Small-angle neutron scattering measurement of block copolymer interphase structure, Polymer, 1983, 24 (9), 1089–1096
Materials: PES was obtained from the chemistry department of Jilin University.
Thomason*, Small-angle neutron scattering measurement of block copolymer interphase structure, Polymer, 1983, 24 (9), 1089–1096
Online since: November 2011
Authors: Hong Yu Wei, Zhong Ning Guo
This paper summaries the research status in application of the orderly function structure and looks into its future development.
Along with the rapid development of detection technology and manufacturing technology, a variety of functional effects of the micro-structured surface have been found, thus constructing or changing the surface micro structure so as to improve the surface properties of materials became a hotspot of current research.
Lotus leaf can be" self-cleaning" because its surface has a large number of micro-nano structure as well as the wax[8].
However, the existing preparation methods can not for industrial production because of low processing efficiency, involving complex chemistry, the demanding experimental conditions, higher cost etc., which make its practical application restricted.
People's diverse needs presents additional challenges for function structure.
Along with the rapid development of detection technology and manufacturing technology, a variety of functional effects of the micro-structured surface have been found, thus constructing or changing the surface micro structure so as to improve the surface properties of materials became a hotspot of current research.
Lotus leaf can be" self-cleaning" because its surface has a large number of micro-nano structure as well as the wax[8].
However, the existing preparation methods can not for industrial production because of low processing efficiency, involving complex chemistry, the demanding experimental conditions, higher cost etc., which make its practical application restricted.
People's diverse needs presents additional challenges for function structure.
Online since: October 2010
Authors: Sergey Kozyukhin, Alexey A. Sherchenkov
It was shown that the structure of these compounds can be represented by stacking of close-packed Te layers.
These results can testify to the more stable structure and thermal properties of GST225 material with annealing.
As determined from XRD measurements, the annealed GST materials have stable hexagonal structures.
The similar behavior has been obtained for GST124 and GST147 structures also, but the changes are less considerable.
The carried out analysis of all stable and metastable GST crystalline structures and fitting of XRD data has shown that the diffraction pattern in Fig.7b cannot correspond only to single-phase structure of GST.
These results can testify to the more stable structure and thermal properties of GST225 material with annealing.
As determined from XRD measurements, the annealed GST materials have stable hexagonal structures.
The similar behavior has been obtained for GST124 and GST147 structures also, but the changes are less considerable.
The carried out analysis of all stable and metastable GST crystalline structures and fitting of XRD data has shown that the diffraction pattern in Fig.7b cannot correspond only to single-phase structure of GST.