Paper Titles
Hydrolysis of S. platensis Using Sulfuric Acid for Ethanol Production
p.451
Adsorptive Removal of Copper from Waste Water Using Biomass & Biochar Based Materials
p.459
Extraction of Essential Oil Form Sweet Lime Orange Peel: A Comparison Study
p.468
The Influencing Factors on the Production of Alcoholic Drinking from Jackfruit (Artocarpus heterophyllus L.)
p.476
Pomelo (Citrus grandis L.) Essential Oil Extraction: A Comparison between Hydrodistillation and Microwave Assisted Hydrodistillation
p.485
Polyphenol, Flavonoid Content and Antioxidant Activity of the Garlic (Allium sativum L.) Extract Obtained by Two Different Extraction Processes
p.493
Production Process of a Nutritional Drink from Mango (Mangifera indica)
p.502
Production Process of a Carbonated Drink from Red Flesh Dragon Fruit (Hylocereus polyrhizus)
p.514
The Initial Study on the Application of Sewage Sludge for Agriculture on the Laboratory Scale
p.524

Pomelo (Citrus grandis L.) Essential Oil Extraction: A Comparison between Hydrodistillation and Microwave Assisted Hydrodistillation

Article Preview

Abstract:

Hydrodistillation (HD) is a traditional technique used in most extraction processes. On the other hand, microwave-assisted hydrogen distillation (MAHD), an advanced method using microwaves in the extraction process, has recently emerged. The chemical ingredients of essential oils obtained from pomelo (Citrus grandis L.) peels obtained by MAHD and by hydrodistillation (HD) were analyzed and compared gas chromatography-mass spectrometry (GC/MS). The results show that there is no significant difference between the two methods in terms of extraction efficiency, at around 4.45 to 4.7%. The main components of essential oils were Limonene, α-pinene, β-Myrcene and Sabinene. The content of those compounds showed no clear quantitative and qualitative difference between HD and MAHD. Experimental results show that the MAHD method provides a good alternative to extracting essential oils from grapefruit, saving time, operating costs and achieving more optimal levels. Keywords: Comparison, Pomelo (Citrus grandis L.), Essential oil, Hydrodistillation, Microwave assist hydrodistillation,

You might also be interested in these eBooks
Advanced Materials and Manufacturing Engineering II View Preview

Info:

Periodical:

Materials Science Forum (Volume 1048)

Pages:

485-492

DOI:

https://doi.org/10.4028/www.scientific.net/MSF.1048.485

Citation:

Cite this paper

Online since:

January 2022

Authors:

Tran Thi Kim Ngan*, Tran Thien Hien, Dao Tan Phat, Ly Thi Ngoc Minh, Huynh Bao Long, Xuan Tien Le

Keywords:

Comparison, Essential Oil, Hydro-Distillation, Microwave Assist Hydrodistillation, Pomelo(Citrus grandis L. )

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

© 2022 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

References

[1] D.T. Phat, T.T. Hien, N.T.C. Quyen, H.T.K. Linh, LN.Y. Trung, V.T. Danh, T.T.L. Ngoc, N.D. Yen, P.M. Quan, and T.T. Quan, Extraction of Essential Oils from Vietnam's Orange (Citrus sinensis) Peels by Hydrodistillation: Modeling and Process Optimization, Asian J Chem 31(2019) 2827-2833.

DOI: 10.14233/ajchem.2019.22178

Google Scholar

[2] T.T.K. Ngan, T.T. Hien, L.X. Tien, T.T. Anh, P.M. Quan, M.H. Cang, N.T.T. Le, V.T. Danh, T.L.N. Yen and T.Q. Toan, Physico-chemical profile of essential oil of Kaffir lime (citrus hystrix DC) Grown in An Giang Province, Vietnam, Asian J Chem. 31(2019) 2855–2858.

DOI: 10.14233/ajchem.2019.22167

Google Scholar

[3] N.T.C. Quyen, T.T.K. Ngan, D.T. Phat and L.T.B. Phuong, Essential Oil Hydrodistillation Process from Vietnamese Calamondin (Citrus microcarpa) Peels and GC/MS Analysis of Essential Oils Components, Asian J. Chem. 31 (2019) 2585-2588.

DOI: 10.14233/ajchem.2019.22148

Google Scholar

[4] N.P. T. Nhan, V.T. Thanh, M.H. Cang, L.T. Duc, C.H. Nguyen, L.T.H. Nhan, T.T. Tran, T.Q Toan and B. L. Giang, Microencapsulation of lemongrass (Cymbopogon citratus) essential oil via spray drying: Effects of feed emulsion parameters, Processes 8 (2020) 40.

DOI: 10.3390/pr8010040

Google Scholar

[5] T.T. Anh, T.D. Le, M.H. Le, T. D. Lam, B.L. Giang, D.C. Nguyen, T.Q. Toan, Effect of drying temperature and storage time on Ocimum gratissimum Linn. leaf essential oil from Central Highlands, Vietnam, Materials Today, Proceedings 18 (2019) 4648–4658.

DOI: 10.1016/j.matpr.2019.07.449

Google Scholar

[6] M.H. Cang, N.D. Dao, T.D. Lam, B.V. Nguyen, D.C. Nguyen and B.L. Giang, Purification Process, Physicochemical Properties, and Fatty Acid Composition of Black Soldier Fly (Hermetia illucens Linnaeus) Larvae Oil JAOCS, J Am Oil Chem Soc 96 (2019) 1303-1311.

DOI: 10.1002/aocs.12263

Google Scholar

[7] L.P. Doan, T.T. Nguyen, M.Q. Pham, Q.T. Tran, Q.L. Pham, D.Q. Tran, V.T. Than and B.L. Giang, Extraction Process, Identification of Fatty Acids, Tocopherols, Sterols and Phenolic Constituents, and Antioxidant Evaluation of Seed Oils from Five Fabaceae Species, Processes 7 (2019) 456.

DOI: 10.3390/pr7070456

Google Scholar

[8] D.T.T. Thuy, T.T. Tuyen, T.T.T. Thuy, P.T.H. Minh, T.Q. Toan, P.Q. Long, D.C. Nguyen, B.L. Giang and N.Q. Chien, Isolation Process and Compound Identification of Agarwood Essential Oils from Aquilaria crassna Cultivated at Three Different Locations in Vietnam, Processes 7 (2019) 432.

DOI: 10.3390/pr7070432

Google Scholar

[9] V.M. Thanh, L.M. Bui, B.L. Giang, N.T. Nguyen, H.T. Thi and T.T.H. Thi, Origanum majorana L. Essential Oil-Associated Polymeric Nano Dendrimer for Antifungal Activity against Phytophthora infestans Materials 12 (2009) 1446.

DOI: 10.3390/ma12091446

Google Scholar

[10] D. T. Phat, D.C. Nguyen, T.T. Hien, V.T. Phan, Q.H. Vu, V.N.D. Viet, N.D. Trinh and B.L Giang, Modeling and optimization of the orange leaves oil extraction process by Microwave-assisted Hydro-distillation: The response surface method based on the central composite approach (RSM-CCD Model) Rasayan, J. Chem 12 (2019) 666-676.

DOI: 10.31788/rjc.2019.1225107

Google Scholar

[11] D. T. Phat, D.C. Nguyen, T.T. Hien and B.L. Giang, Extraction Process of Essential Oil from Plectranthus amboinicus Using Microwave-Assisted Hydrodistillation and Evaluation of It's Antibacterial Activity, Asian J. Chem. 31(2019) 977-981.

DOI: 10.14233/ajchem.2019.21667

Google Scholar

[12] T.T.K. Ngan, N.C. Huong, L.X. Tien and T.T. Anh, Physico-Chemical Characteristics of Rosmarinus officinalis L. Essential Oils Grown in Lam Dong Province, Vietnam, Asian J. Chem. 31 (2019) 2759-2762.

DOI: 10.14233/ajchem.2019.22166

Google Scholar

[13] M.H. Cang, N.D. Chinh, N.P.T. Nhan and B.L. Giang, Physico-Chemical Properties of Sacha Inchi (Plukenetia volubilis L.) Seed Oil from Vietnam, Asian J Chem 32 (2019) 335-338.

DOI: 10.14233/ajchem.2020.22233

Google Scholar

[14] D.T. Phat, H.T. Do, L.Q. Khoi, N.V.G. Phap, M.H. Cang, P.T. Nhut, N.V. Muoi, Evaluation of Physico-Chemical Properties of Lemongrass (Cymbopogon citratus L.) Essential Oil Grown in Tien Giang Province, Vietnam, Asian J Chem 32 (2020) 1248-1250.

DOI: 10.14233/ajchem.2020.22258

Google Scholar

[15] O. Benavente-García, J. Castillo, F.R. Marin, A. Ortuño and J.A. Del Río, Uses and Properties of Citrus Flavonoids, J. Agric. Food Chem 45 (1997) 4505–4515.

DOI: 10.1021/jf970373s

Google Scholar

[16] M.W. Cheong, X.Q. Loke, S.Q. Liu, K. Pramudya, P. Curran and B. Yu, Characterization of volatile compounds and aroma profiles of malaysian pomelo (citrus grandis (l.) osbeck) blossom and peel, J. Essent. Oil Res 23 (2011) 34–44.

DOI: 10.1080/10412905.2011.9700445

Google Scholar

[17] S. Javed, A. Javaid, S. Nawaz, M.K. Saeed, Z. Mahmood, S.Z. Siddiqui and R. Ahmad Phytochemistry, GC-MS Analysis, Antioxidant and Antimicrobial Potential of Essential Oil From Five Citrus Species J. Agric. Sci 6 (2014).

DOI: 10.5539/jas.v6n3p201

Google Scholar

[18] J.S. Baik, S.S. Kim, J.A. Lee, T.H. Oh, J. Y. Kim, N. H. Lee and C.G. Hyun, Chemical composition and biological activities of essential oils extracted from Korea endemic citrus species J Microbiol Biotechnol. 10 (2008) 74–79.

Google Scholar

[19] K. Jaimand, M.B. Rezaee and S. Homami, Comparison Extraction Methods of Essential oils of Rosmarinus officinalis L. in Iran by Microwave Assisted Water Distillation; Water Distillation and Steam Distillation, J Med Plants By-products. 1 (2018) 9–14.

Google Scholar

[20] N. Tigrine-Kordjani, B.Y. Meklati, F. Chemat, Microwave dry, distillation as an useful tool for extraction of edible essential oils, Int J Aromather. 16 (2006) 141–147.

DOI: 10.1016/j.ijat.2006.09.007

Google Scholar

[21] M.M. Jiménez-Carmona, J.L. Ubera, M.D. Luque De Castro, Comparison of continuous subcritical water extraction and hydrodistillation of marjoram essential oil, J Chromatogr A 855 (1999) 625–632.

DOI: 10.1016/s0021-9673(99)00703-7

Google Scholar

[22] M.C. Díaz-Maroto, M.S. Pérez-Coello and M.D. Cabezudo, Supercritical carbon dioxide extraction of volatiles from spices: Comparison with simultaneous distillation-extraction, J Chromatogr A. 947 (2002) 23–29.

DOI: 10.1016/s0021-9673(01)01585-0

Google Scholar

[23] P. Pollien and A. Chaintreau Simultaneous distillation-extraction: Preparative recovery of volatiles under mild conditions in batch or continuous operations, Flavour Fragr J 13(1998) 413–423.

DOI: 10.1002/(sici)1099-1026(199811/12)13:6<413::aid-ffj769>3.0.co;2-h

Google Scholar

[24] M.D. Luque De Castro, M.M. Jiménez-Carmona and V. Fernández-Pérez, Towards more rational techniques for the isolation of valuable essential oils from plants, TrAC - Trends Anal Chem 18 (1999) 708–716.

DOI: 10.1016/s0165-9936(99)00177-6

Google Scholar

[25] E. Reverchon, Supercritical fluid extraction and fractionation of essential oils and related products, J Supercrit Fluids. 10 (1997) 1–37.

DOI: 10.1016/s0896-8446(97)00014-4

Google Scholar

[26] M. Koşar, T. Özek, M. Kürkçüoglu and K.H.C. Başer, Comparison of microwave-assisted hydrodistillation and hydrodistillation methods for the fruit essential oils of foeniculum vulgare, J Essent Oil Res. 19 (2007) 426–429.

DOI: 10.1080/10412905.2007.9699943

Google Scholar

[27] A. Farhat, C. Ginies, M. Romdhane and F. Chemat, Eco-friendly and cleaner process for isolation of essential oil using microwave energy. Experimental and theoretical study, J Chromatogr A. 1216 (2009) 5077–5085.

DOI: 10.1016/j.chroma.2009.04.084

Google Scholar

[28] Z.C. Gazim, L.A. Ana Carolina, A.M.C. Hovell, C.M. Rezende, I.A. Nascimento, G.A. Ferreira and D.A. Garcia Cortez, Seasonal variation, chemical composition, and analgesic and antimicrobial activities of the essential oil from leaves of Tetradenia riparia (Hochst.) Cdd in suthern Brazil, Molecules. 15 (2010) 5509–5524.

DOI: 10.3390/molecules15085509

Google Scholar

[29] F. Conforti, F. Menichini, C. Formisano, D. Rigano, F. Senatore, N.A. Arnold and F. Piozzi, Comparative chemical composition, free radical-scavenging and cytotoxic properties of essential oils of six Stachys species from different regions of the Mediterranean Area Food Chem 116 (2009) 898–905.

DOI: 10.1016/j.foodchem.2009.03.044

Google Scholar

[30] K.H.C. Baser, T. Özek and N. Kirimer, The essential oil of Laser trilobum fruit of Turkish origin, J Essent Oil Res. 5 (1993) 365–369.

DOI: 10.1080/10412905.1993.9698244

Google Scholar

[31] Y. Wang, Z. T. Jiang, and R. Li, Composition Comparison of Essential Oils Extracted by Hydrodistillation and Microwave-assisted Hydrodistillation from Black Pepper (Piper nigrum L.) Grown in China, J. Essent. Oil-Bearing Plants, 12, 2009, 374–380.

DOI: 10.1080/0972060x.2009.10643734

Google Scholar

[32] H. W. Wang, Y. Q. Liu, S. L. Wei, Z. J. Yan, and K. Lu, Comparison of microwave-assisted and conventional hydrodistillation in the extraction of essential oils from mango (Mangifera indica L.) flowers, Molecules, 15, 2010, 7715–7723.

DOI: 10.3390/molecules15117715

Google Scholar

[33] B. Uysal, F. Sozmen, O. Aktas, B.S. Oksal and E.O. Kose, Essential oil composition and antibacterial activity of the grapefruit (Citrus Paradisi. L) peel essential oils obtained by solvent-free microwave extraction: Comparison with hydrodistillation, Int J Food Sci Technol. 46 (2011) 1455–1461.

DOI: 10.1111/j.1365-2621.2011.02640.x

Google Scholar

[34] M.L. Tsai, C.D. Lin, K.A. Khoo, M.Y. Wang, T.K. Kuan, W.C. Lin, Y.N. Zhang, Y.Y. Wang, Composition and bioactivity of essential oil from citrus grandis (L.) Osbeck Mato Peiyu, leaf, Molecules. 22 (2017) 1–19.

DOI: 10.3390/molecules22122154

Google Scholar

[35] N.G. Tao and Y.J. Liu, Chemical composition and antimicrobial activity of the essential oil from the peel of Shatian pummelo (Citrus Grandis Osbeck), Int J Food Prop. 15 (2012) 709–716.

DOI: 10.1080/10942912.2010.500067

Google Scholar

[36] W.O. Okunowo, O. Oyedeji, L.O. Afolabi and E. Matanmi, Essential Oil of Grape Fruit (&amp;lt;i&amp;gt;Citrus paradisi&amp;lt;/i&amp;gt;) Peels and Its Antimicrobial Activities Am, J Plant Sci. 04 (2013) 1–9.

DOI: 10.4236/ajps.2013.47a2001

Google Scholar