Experimental Study on Continuous Preparation of Ultrafine Silicon Nitride Powders in Transport Bed

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Abstract:

Ultrafine e grain amorphous silicon nitride (Si3N4) powders were produced via direct nitridation process of silicon powders in transport bed. The properties of the nitridation products, such as morphology, phase composition, chemical composition and structure, were examined using standard characterization techniques (SEM, XRD, FTIR, etc). The experimental results showed, in the case of silicon powders with particle size of 2.7μm, the conversion rate of silicon was 53.4% at reaction temperature of 1380°C and reaction time of 2.7minutes, and the products mainly comprised amorphous silicon nitride powders.

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14-18

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October 2011

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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[1] N. Karakus, A. O. Kurt, H. O. Toplan: Ceram. Int., vol. 35(2009), p.2381–2385.

Google Scholar

[2] Y. X. Chen, Z. M. Lin, J. T. Li, etc.: J. Eur. Ceram. Soc., vol. 28(2008), p.289–293.

Google Scholar

[3] Y. W. Li, X. Zhang, H. B. Tian, etc.: Bull. Chin. Ceram. Soc., vol. 22(2003), pp.30-34.

Google Scholar

[4] R. Wang, D. H. Li, Y. P. Huang, etc.: China Powder Sci. Technol., vol. 9(2003), pp.35-38.

Google Scholar

[5] S. Y. Shan, J. F. Yang, J. Q. Gao, etc.: J. Inorg. Mater., vol. 21(2006), pp.913-918.

Google Scholar

[6] L. Wang, S. W. Yin, J. C. Dong, etc.: China Patent CN1792774(2006).

Google Scholar

[7] Y. D. Liu, S. Kimura: Powder Technol., vol. 106(1996), pp.160-167.

Google Scholar

[8] X. W. Lv, Study on the Thermal State Experiment and CFD Simulation of Bubbling Fluidized Bed of Synthesis of Si3N4, master's degree thesis. Nanjing University, (2004).

Google Scholar

[9] Z. Jovanovic, S. Kimura, O. Levenspiel: J. Am. Ceram. Soc., vol. 77(1994), pp.186-192.

Google Scholar

[10] D. Campos-Loriz, F. L. Riley: J. Mater. Sci. Lett., vol. 14(1979), pp.1007-1008.

Google Scholar