The Morphology and Phases of Ni-Se Powders Prepared by Hydrothermal Method

Ke Gao Liu; Ya Liu; Bin Xu

doi:10.4028/www.scientific.net/AMM.29-32.1820

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HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vols. 29-32The Morphology and Phases of Ni-Se Powders...

The Morphology and Phases of Ni-Se Powders Prepared by Hydrothermal Method

Abstract:

Ni-Se powders synthesized by hydrothermal co-reduction method from NiCl2.6H2O and SeO2 at 95～220 °C. The phases and morphology of the products were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM) respectively. Experimental results show that, Ni0.85Se can be synthesized at 95～220 °C while noticeable impurities appeared at lower reaction temperatures. The products with single-phase Ni0.85Se obtained at 200 and 220 °C show hollow sphere structures with diameters of about 150 ~ 700 nm, which have complete and regular shape but no holes.

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Periodical:

Applied Mechanics and Materials (Volumes 29-32)

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1820-1823

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https://doi.org/10.4028/www.scientific.net/AMM.29-32.1820

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Online since:

August 2010

Authors:

Ke Gao Liu, Ya Liu, Bin Xu

Keywords:

Hollow Sphere, Hydrothermal Co-Reduction, Nickel Selenides, Semiconductor Materials

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References

[1] Zh.B. Zhuang: Iron, cobalt, nickel, selenium series of liquid-phase regulation of synthesis of compounds, Liquid controlling synthesis of series selenides of Iron, cobalt, nickel (Tsinghua University Comprehensive Papers Training), 2005. 6: 12-26.

Google Scholar

[2] Y. Xie, H. L Su, B. Li, Y. T Qian: Materials Research Bulletin 35 (2000), pp.459-464.

Google Scholar

[3] X. H Liu, N. Zhang, R. Yi, et al: Materials Science and Engineering B 140 (2007), pp.38-43.

Google Scholar

[4] M. Zh. Xue, Zh.W. Fu: Electrochemistry Communications 8 (2006): pp.1855-1862.

Google Scholar

[5] J. Li, Y.C. Zhu, J. Du, et al: Solid State Communications, Vol. 147, Issues 1-2, July 2008, pp.36-40.

Google Scholar

[6] J.G. Yu, H. Tang, Journal of Physics and Chemistry of Solids, Vol. 69, Issues 5-6, May-June 2008, pp.1342-1345.

Google Scholar

[7] N. Zhang, R. Yi, Zh. Wang, et al: Materials Chemistry and Physics, Vol. 111, Issue 1, 15 September 2008: 13-16 Fig. 2 TEM images of Ni-Se powders synthesized at different temperatures a) 220°C b) 200°C c) 180°C d) 150°C b) a) c) d).

Google Scholar

[8] H. Liu, J.Y. Wang: Functional Materials of China, 2000, 31(2), pp.116-123.

Google Scholar

[9] H.M. Cui, H. Liu, X. Li, J. Y Wang: Journal of Solid State Chemistry 177 (2004) , pp.4001-4006.

Google Scholar

[10] H. Liu, H.M. Cui, J.Y. Wang: J. Phys. Chem. B 2004, Vol. 108, pp.13254-13257.

Google Scholar

[11] S.K. Batabyal, C. Basu, A.R. Das, et al: Materials Letters 60 (2006) pp.2582-2585.

Google Scholar

[12] X.H. Liu, G. Zh. Qiu, J. et al: Chemistry Letters Vol. 33, No. 7 (2004), pp.852-853.

Google Scholar