The Synthesis and Characterization of N-Butyl Pyridine Tetrafluoroborate

Abstract:

The halogenated hydrocarbon and pyridine are used in the synthesis of room temperature ionic liquid intermediates chlorinated N-butyl pyridine BPC, and the nuclear magnetic resonance instrument and the intermediate infrared spectrometer are used in chemical structure characterization, so it is determined that the synthesis is the room temperature ionic intermediates BPC. We use differential scanning calorimetric method for the determination of BPC melting point and enthalpy change. We use the double decomposition reaction of BPC and NaBF4 in acetone for the synthesis of BP-BF₄ ionic liquids. We use infrared spectrometer for the structure characterization, it is proved that we have gotten BP-BF₄ room temperature ionic liquids. Solvent polarity and acid alkali both will have an influence on ultraviolet spectrum diagram displacement of room temperature ionic liquid, so in the research of ultraviolet spectrum diagram of ionic liquids and other solvent mixed solution, it is necessary to indicate which solvent is used.

• Periodical: Applied Mechanics and Materials (Volumes 295-298)
• Pages: 236-239
• DOI: https://doi.org/10.4028/www.scientific.net/AMM.295-298.236
• Online since: February 2013
• Authors: Peng Tian, Bo Meng, Hong Bo Zhang, Tian Ling Qin, Yang Yang Song, Zhao Zhao Zhang
• Keywords: BPC-BF₄, Room Temperature Ionic Liquids, UV-Spectrum

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