Research on Multifunctional Gas Chromatography Sample Pretreatment Apparatus

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Abstract:

Multifunctional gas chromatography sample pretreatment apparatus (hereinafter referred to as pretreatment apparatus), which is developed on the basis of gas purge micro-syringe extraction (GP-MSE) technique, is a gas chromatography (GC) sample pretreatment apparatus that integrates extraction, purification, concentration and predissociation. The quantitative and qualitative analysis results analyzed by GC-MS for volatile oil that extracted from the plant samples by steam distillation method and pretreatment apparatus, show that the volatile components extracted by the apparatus outnumber the ones extracted by steam distillation method clearly, and the content of major constituents extracted by the apparatus is higher. The apparatus have advantages of low consumption of agentia, short extraction time, high enrichment efficiency, simple structure, convenience in usage and low operating costs. The apparatus can be widely used in the areas of medicine, agriculture, food, quality control to the sample pretreatment of solid or liquid sample.

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3440-3445

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August 2013

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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[1] Y. Chen, Z. Guo, X. Wang, C. Qiu, J. Chromatogr. A 1184 (2008) 191–219.

Google Scholar

[2] Jeannot M A, Cantwell F F. Solvent microextraction into a single drop [J]. Analytical Chemistry, 1996, 68(13): 2236-2240.

DOI: 10.1021/ac960042z

Google Scholar

[3] Sun S H, Cheng Z H, Xie J P. Identification of volatile basic components in tobacco by headspace liquid-phase microextraction coupled to matrix-assisted laser desorption/ionization with Fourier transform mass spectrometry. Rapid Communications in Mass spectrometry, 2005, 19(8): 1-6.

DOI: 10.1002/rcm.1884

Google Scholar

[4] Zhao R S, Lao W J, Xu X B. Headspace liquid-phase microextraction of trihalomethanes in drinking water and their gas chromatographic determination. Talanta, 2004, 62: 75l-756.

DOI: 10.1016/j.talanta.2003.09.035

Google Scholar

[5] C. Yang, J X. Qiu, C Y. Ren, X F. Piao, D H Li. Gas flow headspace liquid phase microextraction. Journal of Chromatography A 1216, 7694-7699.

DOI: 10.1016/j.chroma.2009.09.039

Google Scholar

[6] C. Yang, X F. Piao, J X. Qiu, C Y. Ren, Xi. Wang, D H Li. Gas purge microsyringe extraction for quantitative direct gas chromatographic-mass spectrometric analysis of volatile and semivolatile chemicals, Journal of Chromatography A, 1218 (2011).

DOI: 10.1016/j.chroma.2011.01.018

Google Scholar

[7] X F. Piao, J H. Bi, C. Yang, X P. Wang, W H. Zhu, D H. Li, Automatic Heating and Cooling System in a Gas Purge Microsyringe Extraction,Talanta, 2011, 86: 142– 147.

DOI: 10.1016/j.talanta.2011.08.047

Google Scholar

[8] Hong Jing Technology Co. , Ltd. STC12C5620AD Microcontroller Devices Using Manual.

Google Scholar

[9] Information on http: /www. stcmcu. com/datasheet/stc/STC-AD-PDF/STC12C5628AD. pdf.

Google Scholar

[10] Texas Instruments Corporation. 12-Bit Micro Power Sampling ANALOG-TO-DIGITAL CONVERTER.

Google Scholar

[11] Information on http: /focus. ti. com. cn/cn/lit/ds/symlink/ads1286. pdf.

Google Scholar

[12] Deutsches Arzneibuch. 1996 (Deutsches Apotheker-Verlag, Stuttgart, Germany, 1996), V. 4. 5. 8.

Google Scholar