Structural State and Mechanical Characteristics of the ZrN Films Prepared by Sputtering

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Abstract:

ZrN films were prepared by magnetron sputtering on die steel substrates. The objective of this study was to investigate the effect of nitrogen flow rate on the microstructure ,morphology, nanohardness properties determined by X-ray diffraction, field-emission scanning electron microscope, nanoindentation, and pin-on-disk, respectively. The XRD shows that ZrN has (111) and (200) preferred orientation under lower nitrogen flow rates. The surface of coatings revealed smaller grains and uniform dense under lower nitrogen flow rates. With increasing the nitrogen flow rates, this result showed ZrN films lead to poor mechanical properties and hardness values. However, films consisted of up high ernitrogen flow rate had much lower friction coefficient.

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9-12

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October 2013

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] B.C. Oberlander, M. Frank and P. Cambell et al.: Thin Sold FilmsVol. 241 (1990), p.222.

Google Scholar

[2] J.A. Garcia, A. Guette, A. Medrano, C. Labrugere, M. Rio, M. Lahays,R. Sanchez, A. Martı́nezand R.J. Rodrı́guez: Vacuum Vol. 64(2002), p.343.

Google Scholar

[3] J.H. Huang, H. Ch. Yang, X.J. Guoand G.P. Yu: Surf. Coat. Technol. Vol. 195(2005), p.204.

Google Scholar

[4] S. Ulrich, C. Ziebert, M. Stqber, E. Nold, H. Holleck, M. Gfken, E. Schweitzer, and P. Schlogmacher: Surf. Coat. Technol. Vol. 188-189 (2004), p.331.

Google Scholar

[5] C.S. Chen, C.P. Liu C.Y.A. Tsao and H.G. Yang: Scr. Mater. Vol. 51 (2004), p.715.

Google Scholar

[6] C.P. Liu and H.G. Yang: Mater. Chem. Phys. Vol. 86(2004), p.370.

Google Scholar

[7] T. Mae, M. Nose, M. Zhou, T. Nagaeand K. Shimamura: Surf CoatTechnol Vol. 142-144(2001), p.954.

Google Scholar