Time-Temperature Effect for Preparation of SnO2 Nanostructures Using Carbon Assisted

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We studied the effect of time and temperature for preparation of SnO2 nanostructures by chemical vapor deposit methods. SnO2 nanostructures were synthesized using Sn powder with carbon charcoal as starting materials. The source materials and Si substrates were heated with various times, temperatures under atmosphere of nitrogen and oxygen. The synthesized products were characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD) techniques. The results showed the nanostructures of prepared products were very uniformly of SnO2 nanowires with diameter about 100-300 nm and length around more 1-2 μm depending on times and temperatures.

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38-41

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October 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] T. Hyeon, Chemical synthesis of magnetic nanoparticles, Chem. Commun. 8 (2003) 927- 934.

Google Scholar

[2] H. Liu, Y. Li, S. Xiao, H. Li, L. Jiang, D. Zhu, B. Xiang, Y. Chen and D. Yu, Control growth of one-dimensional nanostructures of organic materials, J. Phys. Chem. B 108 (2004) 7744-7747.

DOI: 10.1021/jp049455r

Google Scholar

[3] J. Zhu, D. Li, H. Chen, X. Yang, L. Lu and X. Wang, Highly dispersed CuO nanoparticles prepared by a novel quick-precipitation method, Mater. Lett. 58 (2004) 3324-3327.

DOI: 10.1016/j.matlet.2004.06.031

Google Scholar

[4] N.R. Karthikeyan, J. Philip and B. Raj, Effect of clustering on the thermal conductivity of nanofluids, Mater. Chem. and Phys. 109 (2008) 50-55.

DOI: 10.1016/j.matchemphys.2007.10.029

Google Scholar

[5] Q. Kuang, C. Lao, Z.L. Wang, Z, Xie and L. Zhe, High-sensitivity humidity sensor based on a single SnO2 nanowire, J. Am. Chem. Soc. 129 (2007) 6070-6071.

DOI: 10.1021/ja070788m

Google Scholar

[6] J. Pan, H. Shen and S. Mathu, One-dimensional SnO2 nanostructures: synthesis and applications, J. Nanotechnology (2012) 1-12.

Google Scholar

[7] J. Wang, N. Du, H. Zhang, J. Yu and D. Yang, Large-scale synthesis of SnO2 nanotube arrays as high-performance anode materials of Li-ion batteries, J. Phys. Chem. C 115 (2011) 11302-11305.

DOI: 10.1021/jp203168p

Google Scholar

[8] E. Comini, G. Faglia, G. Sberveglieri, Z. Pan, and Z. L. Wang, Stable and highly sensitive gas sensors based on semiconducting oxide nanobelts, Appl. Phys. Lett., 81(10) (2002) 1869-1871.

DOI: 10.1063/1.1504867

Google Scholar

[9] J-H. Park and J-H. Lee, Gas sensing characteristics of polycrystalline SnO2 nanowires prepared by polyol method, Sensors and Actuators B 136 (2009) 151-157.

DOI: 10.1016/j.snb.2008.10.002

Google Scholar

[10] R. Yang, W. Zhao, J. Zheng, X. Zhang and X. Li, One-step synthesis of carbon-coated tin dioxide nanoparticles for high lithium storage, J. Phys. Chem. C 114 (2010) 20272-20276.

DOI: 10.1021/jp107396a

Google Scholar

[11] J.S. Lee, J. Kim and M. Kang, Hydrogen production from ethanol steam reforming over SnO2-K2O/zeolite Y catalyst, Bull. Korean Chem. Soc. 32(6) (2011) 1912-(1920).

DOI: 10.5012/bkcs.2011.32.6.1912

Google Scholar

[12] L. Li, X. Yin, S. Liu, Y. Wang and L. Chen, Taihong Wang, Electrospun porous SnO2 nanotubes as high capacity anode materials for lithium ion batteries, Electrochem. Commun. 12 (2010) 1383-1386.

DOI: 10.1016/j.elecom.2010.07.026

Google Scholar

[13] G-J. Sun, S-W. Choi, S-H. Jung, A. Katoch and S.S. Kim, V-groove SnO2 nanowire sensors: fabrication and Pt-nanoparticle decoration, Nanotechnology 24 (2013) 025504-025512.

DOI: 10.1088/0957-4484/24/2/025504

Google Scholar