Synthesis and Characterization of Nanofibres of 2ZnO·3B2O3·5H2O Ceramic Composite Using the Sol-Gel Processing and the Electrospinning Techniques

Fatih Sevim; Adem Kara; Oguz Aksakal; Fatih Demir; Hayrettin Eroglu

doi:10.4028/www.scientific.net/AMM.749.169

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HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vol. 749Synthesis and Characterization of Nanofibres of...

Synthesis and Characterization of Nanofibres of 2ZnO·3B₂O₃·5H₂O Ceramic Composite Using the Sol-Gel Processing and the Electrospinning Techniques

Abstract:

2ZnO.3B₂O₃.nH₂O (Zinc borate) having the industrially important composite and used as flame retardant, anti-smoke and semiconductor in the electronic circuits was examined different crystal structures. In this study, nanofibers of PVA /zinc nitrate/ boric acid composite were prepared by using sol-gel processing and electrospinning technique. By high temperature calcinations of the above precursor fibers, nanofibers of 2ZnO.3B₂O₃.5H₂O composite with diameters of 110 nm could be successfully obtained. The products have been characterized by X-ray powder diffraction (XRD), thermogravimetry (TG) and differential thermal analysis (DTA), scanning electron microscopy (SEM) and FT-IR (Fourier transform-infrared spectroscopy). The effects of experimental conditions on the products were investigated.

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Periodical:

Applied Mechanics and Materials (Volume 749)

Pages:

169-173

DOI:

https://doi.org/10.4028/www.scientific.net/AMM.749.169

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Online since:

April 2015

Authors:

Fatih Sevim*, Adem Kara, Oguz Aksakal, Fatih Demir, Hayrettin Eroglu

Keywords:

Electrospinning, Nanofibers, Sol-Gel Processing, Zinc Borate Composite

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