Effects of Polishing Direction on the Adhesion Behaviour of Thermal Oxide Scales on AISI 441 Stainless Steel Measured by a Tensile Test

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Abstract:

The tensile test operating in a SEM chamber was applied to investigate the adhesion behaviour of the oxide scale on AISI 441 stainless steel used as interconnect in solid oxide fuel cells (SOFCs). The samples were prepared by aligning the final polishing directions parallel and perpendicular to the tensile loading. The samples were oxidised in water vapour and synthetic air at 800 °C. Changing the final polishing direction from parallel toperpendicular to the loading direction caused the spallation ratio to be increased and reduced the strain initiating the first spallation. Adhesion energiesof scales on the studied samples were in the range of 159-384J.m2.

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413-417

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October 2015

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