Synthesis and Characterization of Thiol Functional Cyclic Carbonate

Wen Cai Li; Huan Huan Zhang; Yan Ling Li; Chang Qing Fu

doi:10.4028/www.scientific.net/AMR.1095.377

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 1095Synthesis and Characterization of Thiol Functional...

Synthesis and Characterization of Thiol Functional Cyclic Carbonate

Abstract:

(2-one-1,3-dioxolan-4-yl) methyl 3-mercaptopropanoate(DMMP), which can be used for Michael addition reaction, was synthesized through two simple routs. First, glycerol carbonate was synthesized under mild conditions without any solvent, using glycerol and dimethyl carbonate as raw materials by green chemistry way. Then DMMP was obtained by simple esterification reaction of glycerol carbonate and 3-mercaptopropionic acid. The structure of them was characterized by 1H NMR and FTIR.

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Advanced Materials Research (Volume 1095)

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377-380

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1095.377

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Online since:

March 2015

Authors:

Wen Cai Li, Huan Huan Zhang, Yan Ling Li, Chang Qing Fu*

Keywords:

Cyclic Carbonate, Glycerol Carbonate, Thiol

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* - Corresponding Author

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