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Effects of Sintering Temperature on the Structure and Conductivity of LiSn2P3O12 Prepared by Mechanical Milling Method

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Abstract:

LiSn2P3O12 has been prepared using mechanochemical milling method and sintered at 700 °C, 800 °C, 900 °C and 1000 °C for 8 hours. All samples sintered up to 900 °C show a rhombohedral structure. However, the sample sintered at 1000 °C possessed a monoclinic structure. This is attributed to the rotation of skeleton LiSn2P3O12 as indicated by the change in the a and c parameters of the sample. The sample sintered at 700 °C shows the highest bulk conductivity of 1.65 × 10-6 S cm-1 and the lowest bulk activation energy of 0.09 eV. The grain boundary activation energy of the samples decreases with increase in sintering temperature due to enhancement in grain contacts.

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Periodical:

Advanced Materials Research (Volumes 129-131)

Pages:

338-342

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.129-131.338

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Online since:

August 2010

Authors:

R. Norhaniza, Ri Hanum Yahaya Subban, Nor Sabirin Mohamed

Keywords:

Conductivity, Nasicon, Sintering, Structure, TiN

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© 2010 Trans Tech Publications Ltd. All Rights Reserved

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References

[1] A. Martinez-Juarez, R. Jimenez, P. Duran-Martin, J. Ibanez and J.M. Rojo: J. Phy: Condense Matter 9 (1997) 4119-4128.

Google Scholar

[2] M.G. Lazarraga, J. Ibanez, M. Tabellout and J. M. Rojo: Composites Science and Technology: 64 (2004) 759-765.

Google Scholar

[3] J.M. Winand, A. Rulmont and P. Tarte: J. Solid State Chemistry 93 (1991) 341-349.

Google Scholar

[4] A. Martinez-Juarez, J.M. Rojo, J. E. Inglesias and J. Sanz: Chem. Mater 7 (1995) 18571862.

Google Scholar

[5] A. Dalvi and K. Shahi: J. Physics and Chemistry of Solids 64 (2003) 813-819.

Google Scholar

[6] J. Alamo: Solid State Ionics 63-65 (1993) 547-561.

Google Scholar

[7] M.E. Medeiros and O. L. Alves: Thermochimica Acta 241 (1994) 33-41.

Google Scholar

[8] A. Martinez-Juarez, C. Pecharroman, J. E. Inglesias and J. M. Rojo: J. Phys. Chem. B 102 (1998) 372-375.

Google Scholar

[9] X.X. Xu, Z. Wen, J. Wu and X. Yang: Solid State Ionics 178 (2007) 29-34.

Google Scholar

[10] C.J. Leo, B.V.R. Chowdari, G.V. Subba Rao and J.L. Souquet: Materials Research Bulletin 37 (2002)1419-1430.

DOI: 10.1016/s0025-5408(02)00793-6

Google Scholar

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