Two-Step Green Hydrothermal Synthesis of ZnO Powders
ZnO2 nanoparticles were synthesized via hydrothermal reaction between Zn5(CO3)2(OH)6 powder and 30 mass% H2O2 aqueous solution at 80 °C for 24 h, and ZnO powders with granular and rodlike morphologies were synthesized via hydrothermal decomposition of the as-synthesized ZnO2 nanoparticles in water at 150-170 °C for 24 h. The obtained products were characterized by X-ray diffraction, Raman and Field emission scanning electron microscopy.
Xiaoming Sang, Pengcheng Wang, Liqun Ai, Yungang Li and Jinglong Bu
L. Liu et al., "Two-Step Green Hydrothermal Synthesis of ZnO Powders", Advanced Materials Research, Vols. 284-286, pp. 654-657, 2011