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A Single-Step Synthesis of Rutile TiO2 Dendrite Crystal with Sonication

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Abstract:

A single-step sonochemical method to directly prepare rutile nanocrystal TiO2 has been developed. TiO2 nanaoparticles were synthesized by the hydrolysis of TiCl4 in the presence of water and ethanol under ultrasonic irradiationat 70 °C for 3 h. The crystalline forms and crystallite sizes of the produts were characterized by X-ray diffraction, transmission electron microscopy and thermogravimetry-differential thermal analysis. The TEM images showed the morphology of as-prapared TiO2 was pinnate in shape and the average sizes were ca. 4/12 nm (W/L). The columnar particles were linked together each other at the certain principle, forming the shape like dendrite crystal. The formation mechanism of the dendrite crystal nanocrystalline TiO2 was also discussed.

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Periodical:

Advanced Materials Research (Volumes 356-360)

Pages:

399-402

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.356-360.399

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Online since:

October 2011

Authors:

Xi Kui Wang, Wei Lin Guo, Chen Wang

Keywords:

Dendrite Crystal, Rutile TiO2, Sonication, Synthesis

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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References

[1] B. Samuneva, V. Kozhukharqv, C. Trapalis and R. Kranold: J. Mater. Sci. Vol.28(1993), p.2353

Google Scholar

[2] H. Cheng, J. Ma, Z. Zhao and L.Qi: Chem. Mater. Vol.7(1995) , p.663

Google Scholar

[3] S. Peres-Durand, J. Rouviere and C.Guizard: Colloids and Surfaces A: Physicochem. Eng. Aspects Vol.98(1995) , p.251

Google Scholar

[4] H. Kominami, J. Kato, Y. Takada: Cata. Lett. Vol.46(1997) , p.265

Google Scholar

[5] N. A. Dhas and K.S. Suslick: J. Am. Chem. Soc. Vol.127(2005) , p.2368.

Google Scholar

[6] W. H. Suh, A.R. Jang, Y.H. Suh and K.S. Suslick: Adv. Mater. Vol.18(2006) , p.1832.

Google Scholar

[7] E. B. Flint and K. S. Suslick: Science Vol.253(1991) , p.1397.

Google Scholar

[8] Y. T. Didenko, W. B. McNamara II and K.S. Suslick: J. Am. Chem. Soc. Vol.121 (1999) , p.5817

Google Scholar

[9] D. L. Chen and L. Gao: J. Crystal Growth Vol.264(2004) , p.216

Google Scholar

[10] Y. Zhu, X. Wang, W. Guo, J. Wang and C. Wang: Ultrason. Sonochem. Vol.17(2010) , p.675

Google Scholar

[11] Y. Zheng, E. Shi and W. Li: Sci. in China (series E) Vol. 31(2001) , p.204

Google Scholar

[12] J. Zhao, Z. Wang and Y. Liu: Chem. J. Chinese Universities Vol. 20(1999) , p.467

Google Scholar

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