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Preparation for Nano-NiO by Electrolysis of Nickel in HOCH2CH2OH Solution

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Abstract:

A method to prepare nickel oxide material which has a high purity and nano-sized particle was developed. nano NiO was synthesized by sol-gel method using nickel alkoxide as precursors. The structural characterization of the obtained materials was performed by thermal analysis TG-DTA, X-ray diffraction (XRD), Laser Raman spectra and Transmission Electron Microscopy (TEM). The characterization results indicated that NiO nano-particles (size 25–35 nm) are obtained by hydrolyzing of metal alkoxide of Ni(OCH2CH2OH)2 and possess high purity.

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Periodical:

Advanced Materials Research (Volumes 399-401)

Pages:

593-596

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.399-401.593

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Online since:

November 2011

Authors:

Chuan Gao Zhu, Feng Wu Wang

Keywords:

Electrolysis, HOCH2CH2OH, Nano NiO, Nickel Alkoxide Complex

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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