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Preparation of Silica Nano-Rods by CVD
Abstract:
The straight silica nano-rods with a diameter of about 200nm and smooth surface were synthesized by chemical vapor deposition method at 1300°C. The as-synthesized samples were characterized by means of scanning electron microscopy, energy dispersive x-ray, and transmission electron microscopy. The results show that as-synthesized silica nano-rods have a uniform size, well-defined shape, and smooth surface. However, the morphologies and microstructures of silica nano-rods are affected by synthesis conditions, such as the concentration of the SiOx and the the deposition temperature. On the basis of these experimental results, a possible growth mechanism of silica nano-rods in this process is proposed.
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359-362
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Online since:
June 2008
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© 2008 Trans Tech Publications Ltd. All Rights Reserved
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