Synthesis of Nanocrystalline Fe25Al57.5Ni17.5 by Mechanical Alloying

Qi Zhi Cao; Jing Zhang

doi:10.4028/www.scientific.net/AMR.476-478.1318

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 476-478Synthesis of Nanocrystalline Fe25Al57.5Ni17.5 by...

Synthesis of Nanocrystalline Fe₂₅Al_57.5Ni_17.5 by Mechanical Alloying

Abstract:

Nanostructured Fe25Al57.5Ni17.5intermetallics was prepared directly by mechanical alloying (MA) in a high-energy planetary ball-mill. The phase transformations and structural changes occurring in the studied material during mechanical alloying were investigated by X-ray diffraction (XRD). Thermal behavior of the milled powders was examined by differential thermal analysis (DTA). Disordered Al(Fe,Ni) solid solution was formed at the early stage. After 50 h of milling, Al(Fe,Ni) solid solution transformed into Al3Ni2，AlFe3，AlFe0.23Ni0.77 phase. The power annealed at temperature 500 results in forming of intermetallics AlFe3 and FeNi3 after 5h milling. The nanocrystalline intermetallic compound was obtained after 500h milling.

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Periodical:

Advanced Materials Research (Volumes 476-478)

Pages:

1318-1321

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.476-478.1318

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Online since:

February 2012

Authors:

Qi Zhi Cao, Jing Zhang

Keywords:

Intermetallic, Mechanical Alloying, X-Ray Diffraction (XRD)

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