Solid-Solid Reaction Preparation for Nanoparticles of Bioinorganic Complex of Bismuth and Serine at Room Temperature

Abstract:

Nanoparticles of the bioinorganic complex of bismuth and serine can be prepared very easily by a room temperature solid-solid reaction with the raw materials of bismuth triiodide and serine. The complex is characterized by elemental analysis, X-ray powder diffraction and transmission electron micrograph. The characterizations indicate that the composition of the complex is Bi[I(HOCH₂CHNH₂COO)]_1.5. The crystal structure of the complex belongs to orthorhombic system with the lattice parameters: a = 0.8355 nm, b = 1.8688 nm and c = 2.2511 nm. The average diameter of the bioinorganic complex nanoparticles is about 40 nm.

• Periodical: Advanced Materials Research (Volume 549)
• Pages: 292-296
• DOI: https://doi.org/10.4028/www.scientific.net/AMR.549.292
• Online since: July 2012
• Authors: Guo Qing Zhong, Rong Rong Jia, Yu Qing Jia
• Keywords: Bioinorganic Complex of Bismuth, Bioinorganic Complex of Serine, Nanoparticle, Room Temperature Solid- Solid Reaction, X-Ray Diffraction (XRD)

References

[1] G. Cantos, C.L. Barbieri, M. Iacomini, P.A.J. Gorin and L.R. Travassos: Biochem. J. Vol. 289 (1993), p.155.

[2] L. Dawara and R.V. Singh: J. Coord. Chem. Vol. 64 (2011), p.931.

[3] G.Q. Zhong, S.R. Luan, P. Wang, Y.C. Guo, Y.R. Chen and Y.Q. Jia: J. Therm. Anal. Cal. Vol. 86 (2006), p.775.

[4] P. Kopf-Mair and T. Klapotka: Inorg. Chim. Acta. Vol. 49 (1988), p.152.

[5] Z.P. Zhang, G.Q. Zhong and Q.Y. Jiang: Prog. Chem. Vol. 20 (2008), p.1315.

[6] D.C. Reis, M.C.X. Pinto, E.M. Souza-Fagundes, S.M.S.V. Wardell, J.L. Wardell and H. Beraldo: Eur. J. Med. Chem. Vol. 45 (2010), p.3904.

[7] Q.Y. Jiang, J. Shen and G.Q. Zhong: Prog. Chem. Vol. 18 (2006), p.1634.

[8] M. Mehring: Coord. Chem. Rev. Vol. 251 (2007), p.974.

[9] N. Yang and H.Z. Sun: Coord. Chem. Rev. Vol. 251 (2007), p.2354.

[10] N.N. Greenwood and A. Earnshaw: Chemistry of the Elements (second edition, Reed Educational and Professional Publishing Ltd., Oxford 1997).

[11] R.R. Jia, C.P. Wu, Y.X. Yang, Y.R. Chen, J.R. Zhang and Y.Q. Jia: Amino Acids Vol. 28 (2005), p.409.

[12] R.R. Jia, C.P. Wu, S. Wu, Y.X. Yang, Y.R. Chen and Y.Q. Jia: Amino Acids Vol. 31 (2006), p.85.

[13] S.R. Luan, Y.H., Zhu and Y.Q. Jia: Protein & Peptide Letters Vol. 15 (2008), p.1094.