Study on Synthesis Technology of Glyoxylic Acid Fine Chemicals

Shu Xin Zhang

doi:10.4028/www.scientific.net/AMR.573-574.145

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Study on Synthesis Technology of Glyoxylic Acid Fine Chemicals
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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 573-574Study on Synthesis Technology of Glyoxylic Acid...

Study on Synthesis Technology of Glyoxylic Acid Fine Chemicals

Abstract:

Glyoxylic acid is an important intermediate of organic chemical and it can generate dozens of fine chemical products. At present, its production process is mostly in the manufacturing of 30% to 50% solution of glyoxylic acid. Due to the presence of large amounts of water, solution of glyoxylic acid in aqueous solution is difficult to meet the needs of medicine, food and other industries which require high-purity crystal glyoxylic acid products. The experiments show that synthesis process using crystal glyoxylic acid as raw material in the manufacturing of allantoin instead of solution of glyoxylic acid is reasonable and feasible. Compared with other synthetic methods reported in the literature, this method has advantages of simple technology and high yielding. Solvent inspection results show that solvent polarity has some influence on the reaction results. That the polarity is too strong and too weak is not conducive to reaction. The mixed solution of tetrahydrofuran and ethanol is suitable reaction solvent.

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Periodical:

Advanced Materials Research (Volumes 573-574)

Pages:

145-149

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.573-574.145

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Online since:

October 2012

Authors:

Shu Xin Zhang

Keywords:

Fine Chemicals, Glyoxylic Acid, Technology

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References

[1] Alardin F, Wullens H, Hermans, et. al. Mechanistic and Kinetic Studies on Glyoxal Oxidation with Bi-and Pb-promoted Pd/C Catalysts . J Mol Catal A, 2005, 223: 79-82.

DOI: 10.1016/j.molcata.2004.08.030

Google Scholar

[2] Laura P, Francesca P. Oxidation of Alcohols and Sugars Using Au/C Catalysts Part 1 Alcohols. App Catal A: Gen, 2005, 291: 199-203.

Google Scholar

[3] Aurore D, Sophie H, Michel D. Bimetallic Bi-Pt, Ru-Pt and Ru-Pd and Trimetallic Catalysts for the Selective Oxidation of Glyoxal into Glyoxalinc Acid in Aqueous Phase. Appl Catal A: Gen. 2005, 282: 303-306.

DOI: 10.1016/j.apcata.2004.12.023

Google Scholar

[4] Monsanto Company, Ozonization and Reduction of Unsaturated Organic Compounds, US 3145232, 1964-8-18.

Google Scholar

[5] R A Poole&Co. (Stainless) LTD. Producing Carbonyl Compounds by Anozonization Reduction Process . GB 1092615, 1967-11-29.

Google Scholar