Effects of Sintering Temperature on Microstructure and Phase Formation of Nitrides Bonded MgAl2O4-Crefractory

Article Preview

Abstract:

The microstructure and phase analysis of in situ nitrides formation in MgAl2O4-C refractory were investigated with different temperature. The phase compositions and microstructure of the MgAl2O4-C refractory were investigated by X-ray diffraction (XRD) and scanning electron microscope (SEM). The results show that sintering temperature has a significant influence on the microstructure and phase analysis of MgAl2O4 refractory. As the sintering temperatures are 1450°C and 1500°C, nitride that formed in samples is β-Sialon and the crystal morphology is columnar with short size. With the temperature rise to 1550°C and 1600°C, nitride formed in sample is AlON with the crystal morphology is tabular polymorph with large size.

You might also be interested in these eBooks

Info:

Periodical:

Advanced Materials Research (Volumes 634-638)

Pages:

2354-2357

Citation:

Online since:

January 2013

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2013 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] M. Sharuif, M.A. Faghihi-Sani, F. Golestani-Fard, A. Saberi, Ali Khalife Soltani: J. Alloy. Compd. Vol. 74-77 (2010), p.500.

Google Scholar

[2] Z. Ali Nemati, Pouya Moetakef: Comp. Mater. Sci. Vol. 723-728 (2007), p.39.

Google Scholar

[3] Yeh, C.L., Wu, F.S., Chen, Y.L.: J. Alloy. Compd. Vol. 3985–3990 (2011), p.509.

Google Scholar

[4] Enquan He, Jianshe Yue, Lei Fan, Chao Wang, Hongjie Wang: Scripta Mater. Vol. 155–158 (2011), p.65.

Google Scholar

[5] Frank, L.R.: J. Am. Ceram. Soc. Vol. 245 (2000), p.83.

Google Scholar

[6] Ekstrom, T., Nygren, M.: J. Am. Ceram. Soc. Vol. 259 (1992), p.75.

Google Scholar

[7] N.D. Corbin: J. Eur. Ceram. Soc. Vol. 5 (1989), p.143.

Google Scholar

[6] H. X. Willems, M. M. R. Hendrix, G. D. With, R. Metselaar: J. Eur . Ceram. Soc. Vol 10(1992), p.339.

Google Scholar

[7] L. Kaufman: CALPHAD, 3(1979), p.275.

Google Scholar