Alcohol Interchange Synthesis of a Novel Titanium Glycolate

Guo Liang Shen; Gui Ling Ning

doi:10.4028/www.scientific.net/AMR.634-638.638

Paper Titles

Synthesis of Three-Dimensionally Ordered Macroporous Co/SiO₂ Catalysts by Sol-Gel Method
p.620

Vanadium-Chromium Oxide: Effective Catalysts for Ammoxidation of 3-Picoline
p.624

Catalytic Synthesis of Ethyl Acetate Using Ti₂SnC
p.628

Study on α-Pinene Isomerization over MCM-41 Supported SO₄^2-⁄TiO₂
p.632

Alcohol Interchange Synthesis of a Novel Titanium Glycolate
p.638

Esterification of 5-Norbornene-2,3-Dicarboxylic Anhydride under Titanium Catalyst
p.642

Esterification of Menthol and Lactic Acid by Silicotungstic Acid Catalyst Supported on Bentonite
p.647

Inhibition Effect of N-Octyl-2-Pyrrolidonium Chloride on the Corrosion of Mild Steel in Acidic Medium
p.651

Inhibitory Kinetics of Isooctyl 4-Hydroxy-3-Methoxycinnamate on Tyrosinase-Catalyzing Reaction
p.655

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Alcohol Interchange Synthesis of a Novel Titanium Glycolate

Abstract:

A much simpler and more straightforward method, alcohol interchange for the synthesis of titanium glycolate has been suggested. The method implied the reaction of tetraethyl orthosilicate with ethylene glycol on heating in air. The thermal property of titanium glycolate was characterized by thermal gravimetric (TG) and Differencial Thermal Analysis (DTA) analysis. X-ray diffraction (XRD) was used to confirm the conversion of crystalline phase of titanium glycolate from anatase to rutile. The characterization of titanium glycolate and products of its pyrolysis was conducted using scanning electron microscopes.