The Microwave Synthesis and Photocatalytic Activity of ZnO/TiO2 Nanocomposites

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ZnO/TiO2 nanocomposites were prepared by mixing of ultrasonic vibration and sintering at 500°C for 2 h initial nano-ZnO and nano-TiO2 which were synthesized by a microwave irradiation heating technique from an aqueous solution of Zn(Ac)22H2O, Ti(SO4)2, respectively. The samples were characterized by the techniques of X-ray diffraction (XRD) and transmission electron microscopy (TEM). And we have also carried on research to the photocatalytic activity of the as-prepared ZnO/TiO2 nanocomposites by photo-degrading methyl orange. The result indicates that the as-prepared sample is a good photocatalyst. When m (TiO2) /m (ZnO) ratio was equal to 4, the photocatalytic activity of the nanocomposites is best. The result shows that the degradation ratio of the methyl orange (2mg/L) has reached 93% within 80 min

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187-192

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January 2013

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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[1] J Yang, D Li, X Wang, X J Yang, L D Lu. Rapid synthesis of nanocrystalline TiO2/SnO2 binary oxides and their photoinduced decomposition of methyl orange. J solid State Chemistry, 165(1)(2002)193-198.

DOI: 10.1006/jssc.2001.9526

Google Scholar

[2] Z Y Wang, S W Ding, M H Zhang, Y Z Zhang. Self-assembled synthesis and photocatalysis of nano-TiO2-ZnO mesoporous meterial. Acta Chimica sinica, 63(3) (2005)243-248.

Google Scholar

[3] T V Nguyen, O B Yang. Photoresponse and A C impedance characterization of TiO2-SiO2 mixed oxide for photocatalytic water decomposition. Catalysis Today. 87 (2003)69-75.

DOI: 10.1016/j.cattod.2003.10.014

Google Scholar

[4] M Kang, S J Choung, Y P Jong. Photocatalytic performance of nanometersized FexOy/TiO2 particle synthesized by hydrothermal method. Catalysis Today. 87(2003)87-97.

DOI: 10.1016/j.cattod.2003.09.011

Google Scholar

[5] X Z Li, F B Li, C L Yang, et al. Photocatalytic activity of WOx-TiO2 under visible light irradiation. Journal of Photochemistry and photobilogy A; Chemistry. 141(2001)209-217.

DOI: 10.1016/s1010-6030(01)00446-4

Google Scholar