Development of Electroless Ni-P-ZrO2 Nanocomposite Coatings by Codeposition of Mechanically Reduced ZrO2 Nanoparticles

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In this study, an attempt has been made to develop electroless Ni-P-ZrO2 nanocomposite coatings on mild steel substrate where the reinforced nanosized ZrO2 particles were prepared by mechanical milling using high energy planetary ball mill. An alkaline bath was used with a suspension of ZrO2 particles (4 g/L) for the synthesis of Ni-P-ZrO2 composite coating. The surface morphology, size range and phase analysis of as-prepared ZrO2 particles were characterized using X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), and the properties of the coatings such as hardness and wear (ball-on-disc) were investigated and compared with Ni-P deposits. The results showed that as-prepared ZrO2 particles exhibit irregular shaped and size ranges from 14 to 17nm. After heat treatment (400°C,1h), the microhardness and wear resistance of the coatings are significantly improved. The Ni-P-ZrO2 nanocomposite coatings exhibit enhanced wear resistance over NiP coating.

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545-549

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August 2013

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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