Synthesis and Millimeter Wave Attenuation Properties of the FeCl3-Graphite Intercalation Compound

Ming Shan Zhou; Yong Ming Zhang

doi:10.4028/www.scientific.net/AMR.750-752.908

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 750-752Synthesis and Millimeter Wave Attenuation...

Synthesis and Millimeter Wave Attenuation Properties of the FeCl₃-Graphite Intercalation Compound

Abstract:

The graphite intercalation compound with large exfoliated volume was prepared by chemical oxidation method. The experimental parameters on the exfoliated volume were discussed in detail. It was found that the optimum preparing conditions went as follows: the mass ratio of graphite flakes:C₂H₅COOH:FeCl₃:CrO₃=1:2.8:0.3:0.2, the reaction temperature and time were 30 °C and 40 minutes, respectively. The exfoliated volume of GIC reached up to 575 mL·g¹ in the conditions. The composition, structure and properties of the graphite intercalation compound were characterized and analyzed by SEM, TG, DSC, VSM techniques. The millimeter wave (MMW) attenuation performances of GIC were investigated by MMW radar measurement device. The results showed that the MMW attenuation properties of FeCl₃-GIC are batter than H₂SO₄-GIC because of its magnetic absorption for millimeter wave.

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Advanced Materials Research (Volumes 750-752)

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908-913

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https://doi.org/10.4028/www.scientific.net/AMR.750-752.908

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August 2013

Authors:

Ming Shan Zhou, Yong Ming Zhang

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Exfoliated Graphite (EG), Exfoliated Volume, Graphite Intercalation Compound (GIC), Millimeter Wave (MMW)

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