Annealing Temperature Dependent on Microstructure and Ethanol Gas Sensing Properties of TiO2Thin Films

Article Preview

Abstract:

The TiO2 thin films were prepared by a dc reactive magnetron sputtering technique from high purity Ti target on silicon (100) wafers and alumina substrates inter-digital with gold electrodes. The as-deposited films were annealed from 400°C up to 800°C with 100 °C steps for 1 hour in air ambience in order to promote microstructure, morphology and gas-sensing properties. The change in microstructure and morphology of the films were investigated by X-ray diffraction (XRD) and field emission scanning electron microscopy (FE-SEM). The enhancement in the gas-sensing properties was test by ethanol gas. The prepared thin films were exposed to ethanol gas at concentration 1,000 ppm in purify dry air carrier. The resistance was measured as a function of the ethanol concentration of the films at operated temperatures in the range of 250 - 350°C. The influence of annealing temperature at 500 °C of TiO2 thin film has a highest sensitivity at 350 °C operated temperature.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

213-216

Citation:

Online since:

September 2013

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2013 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] S. Sankar and K.G. Gopchandran, Effect of annealing on the structural, electrical and optical properties of nanostructured TiO2 thin film, Cryst. Res. Technol. 44. No. 9 (2009) 989-994.

DOI: 10.1002/crat.200900073

Google Scholar

[2] S. Hsiao, J. Lin, Y. Chin, Comparison of sol-gel and sputtering method properties of TiO2 thin film ultraviolet sensor, IEEE Sensors. (2008) 321-324.

DOI: 10.1109/icsens.2008.4716446

Google Scholar

[3] P. Eiamchai, P. Chindaudom, A. Pokaipisit and P. Limsuwan, A spectroscopic ellipsometry study of TiO2 thin films prepared by ion-assisted electron-beam evaporation, Curr. Appl. Phys. 9 (2009) 707-712.

DOI: 10.1016/j.cap.2008.06.011

Google Scholar

[4] A. Wisitsoraat, C. Promjuntuk, V. Patthanasettakul and A. Tuantranont, Gas sensing characterization of Ion-Assisted E-beam evaporated TiO2 thin films with nanometer scale thickness, ECTI-CON. (2007) 191-193.

Google Scholar

[5] M. Horprathum, P. Eiamchai, P. Chindaudom, N. Nuntawong, V. Patthanasettakul, P. Limnonthakul and P. Limsuwan, Characterization of inhomogeneity in TiO2 thin films prepared by pulsed dc reactive magnetron sputtering, Thin Solid Films. 520 (2011) 272-279.

DOI: 10.1016/j.tsf.2011.07.064

Google Scholar

[6] M. Horprathum, P. Chindaudom, P. Limnonthakul, P. Eiamchai, N. Nuntawong, V. Patthanasettakul, A. Pokaipisit and P. Limsuwan, Dynamic in situ spectroscopic ellipsometric study in inhomogeneous TiO2 thin-film growth, J. Appl, Phys. 108 (2010) art. No. 013522.

DOI: 10.1063/1.3457839

Google Scholar

[7] M. Horprathum, K. Limwichean, A. Wisitsoraat, P. Eiamchai, K. Aiempanakit, P. Limnonthakul, N. Nuntawong, V. Pattantsetakul, A. Tuantranont, P. Chindaudom, NO2-sensing properties of WO3 nanorods prepared by glancing angle DC magnetron sputtering, Sensors and Actuators B. 176 (2013) 685– 691.

DOI: 10.1016/j.snb.2012.09.077

Google Scholar