The Hydrothermal Synthesis of ZrO2 Nanoparticles and their Optical Absorption Properties

Xiao Ming Fu

doi:10.4028/www.scientific.net/AMR.873.164

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 873The Hydrothermal Synthesis of ZrO2 Nanoparticles...

The Hydrothermal Synthesis of ZrO₂ Nanoparticles and their Optical Absorption Properties

Abstract:

ZrO₂ nanoparticles with a diameter range of less than 10 nm are successfully synthesized with zirconium nitrate as zirconium source and stronger ammonia water as precipitant at 210 °C for 48 h via the easy hydrothermal method. The phase, the morphologies and optical absorption properties of the samples have been characterized and analyzed by X-ray diffraction (XRD), field-emission transmission electron microscopy (TEM) and ultraviolet-visible absorption spectroscopy (UV-VIS), respectively. XRD analysis shows that the phase of as obtained samples is ZrO₂. TEM analysis confirms that using stronger ammonia water as precipitant instead of NaOH and the increase of the reaction temperature are in favor of the synthesis of ZrO₂ nanoparticles. And UV-VIS measurements show that ZrO₂ nanoparticles have a good optical absorption property.

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Advanced Materials Research (Volume 873)

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164-167

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https://doi.org/10.4028/www.scientific.net/AMR.873.164

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Online since:

December 2013

Authors:

Xiao Ming Fu*

Keywords:

Hydrothermal Method, Optical Absorption Property, Stronger Ammonia Water, Zirconium Nitrate, ZrO₂ Nanoparticles

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