Quantitative Phase Analyses of a Slag Using X-Ray Powder Diffraction

Wei Jin Zeng; Chao Zeng; Wei He

doi:10.4028/www.scientific.net/AMR.881-883.1241

Paper Titles

Research on Compressive Properties of Sea Sand Concrete
p.1221

Well Pattern Optimization Design for CBM Development
p.1225

Heat Transfer Analysis and Energy-Saving Methods of the Exterior Windows in the Northern Area
p.1233

The Influence of Pretreatment and Usage on the Humidity Control Property of a Novel Paperboard
p.1237

Quantitative Phase Analyses of a Slag Using X-Ray Powder Diffraction
p.1241

The Impact of λ/4 Type Absorber Protective Layer 's Thickness on Absorbing Properties
p.1245

Experiment on Decarburization of High Carbon Fly Ash and Preparation of Concrete
p.1250

The Research of Hardox400 HSLA Steels Weldability
p.1257

Surface Modification of SS2205 Duplex Stainless Steel by Plasma Nitriding at Anodic Potential
p.1263

HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 881-883Quantitative Phase Analyses of a Slag Using X-Ray...

Quantitative Phase Analyses of a Slag Using X-Ray Powder Diffraction

Abstract:

The quantitative phase analyses of a slag have been successfully carried out by using both of the full-profile Rietveld and RIR methods from X-ray powder diffraction data. The qualitative phase analysis indicates that the slag contains mayenite (CaO)₁₂(Al₂O₃)₇, olivine Ca₂(SiO₄), gehlenite Ca₂Al (AlSiO₇), lemite Ca₂(SiO₄) and hibonite CaO(Al₂O₃)₆. The quantitative analysis from Rietveld refinement shows that the weight concentrations of mayenite, olivine, gehlenite, lemite and hibonite for the slag are 48.8(4) wt.%, 32.2(5) wt.%, 11.0(9) wt.%, 6.2(1.1) wt.% and 1.8 (1.2) wt.%, respectively. The quantitative phase analysis results obtained by Rietveld method are more precise then those by RIR method.

You might also be interested in these eBooks

Chemical, Material and Metallurgical Engineering III

View Preview

Info:

Periodical:

Advanced Materials Research (Volumes 881-883)

Pages:

1241-1244

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.881-883.1241

Citation:

Cite this paper

Online since:

January 2014

Authors:

Wei Jin Zeng, Chao Zeng, Wei He*

Keywords:

Quantitative Phase Analysis, Rietveld Method, Slag, X-Ray Powder Diffraction

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

* - Corresponding Author

References

[1] D. L. Bish, and J. E. Post, Quantitative mineralogical analysis using the Rietveld full-pattern method, Am. Mineral. Vol. 78, (1993), p.932–940.

Google Scholar

[2] D. L. Bish, and S. A. Howard, Quantitative mineralogical analysis using the Rietveld method, J. Appl. Crystallogr. Vol. 21, (1988). P. 86–91.

DOI: 10.1107/s0021889887009415

Google Scholar

[3] S. S. Iyengar, N. V. Phadnis, and R. Suryanarayanan, Quantitative analyses of complex pharmaceutical mixtures by the Rietveld method, Powder Diffr. Vol. 16, (2001), p.20–24.

DOI: 10.1154/1.1332076

Google Scholar

[4] Jade6. 0, XRD Pattern Processing Materials, Data Inc., (2005).

Google Scholar

[5] PDF-2 2011 (Database), edited by Dr. Soorya Kabekkodu, International Centre for Diffraction Data, Newtown Square, PA, USA. (2011).

Google Scholar

[6] R.A. Young, A.C. Larson, and C.O. Paiva-Santos, User's Guide to Program DBWS-9807a for Rietveld Analysis of X-Ray and Neutron Powder Diffraction Patternswith a PC and Various Other Computers, School of Physics, Georgia Institute of Technology, Atlanta, Georgia. (2000).

Google Scholar

[7] H. Bartl, T. Scheller, Zeitschrift fuer Kristallographie, Kristallgeometrie, Kristallphysik, Kristallchemie Vol. 95 (1936), pp.175-175.

Google Scholar

[8] S. Udagawa, K. Urabe, M. Natsume, T. Yano,: Cement and Concrete Research, Vol. 10 (1980), pp.139-144.

DOI: 10.1016/0008-8846(80)90070-8

Google Scholar

[9] M. Kimata, N. Ii: Neues Jahrbuch fuer Mineralogie. Abhandlungen (Band-Nr), Vol. 144 (1982), pp.254-267.

Google Scholar

[10] K.H. Jost, B. Ziemer, R. Seydel: Acta Crystallogr. B Vol. 33 (1977), pp.1696-1700.

Google Scholar

[11] A. Utsunomiya, K. Tanaka, H. Morikawa, F. Marumo, H. Kojima: J. Solid State Chem. Vol. 75 (1988), pp.197-200.

DOI: 10.1016/0022-4596(88)90317-9

Google Scholar