Study of Material Properties for Microwave Assisted Digestion of Fallopia Multiflora for Multielement Analysis by ICP-AES

Article Preview

Abstract:

In this work, the contents of all elements including Cu, Fe, Zn, Al, Mn, Cd, Pb, Ti and As were tested by ICP-AES technique, which elements root in Fallopia multiflora from different place such as Renhe county, Miyi county, Qianjiang county and so on. Detection limits ranged 0.0021ug/ml-1 and 0.076ug/ml-1, the relative standard deviations for all these elements were lower than 2%, and recovery rates ranged 95.52% and 107.2%. The consequence showed that there were many metallic elements in Fallopia multiflora from different places; contents of Fe and Al were highest in Renhe county’s sample specially; contents of Mn, Cu, Zn and Ti were moderately high in Yanbian county specially; and contents of As, Cd and Pb were lowest in Qianjiang county. concentrations of elements within Fallopia multiflora from different places were different, which may have some relations with the environment where Fallopia multiflora grew. So ,its necessary to monitor the environment condition of plant surronding.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

15-18

Citation:

Online since:

June 2014

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] Zheng C J, Zhao S J, Zhao Z H, et al. Molecular authentication of the traditional medicinal plant Fallopia multiflora[J]. Planta medica, 2009, 75(08): 870-872.

DOI: 10.1055/s-0029-1185382

Google Scholar

[2] Yan H J, Fang Z J, Fu J, et al. The Correlation Between Bioactive Components of Fallopia multiflora Root and Environmental Factors[J]. The American journal of Chinese medicine, 2010, 38(03): 473-483.

DOI: 10.1142/s0192415x10007993

Google Scholar

[3] Anderson K A. Micro-digestion and ICP-AES analysis for the determination of macro and micro elements in plant tissues[J]. Atomic spectroscopy, 1996, 17(1): 30-33.

Google Scholar

[4] Yi Jun-Peng, Yin Yong, Li Xin. Trace Elements Determination Methods for Foods. Journal of Henan university of science and Technology (Natural Science), 2004, 25(5): 89-92.

Google Scholar

[5] Wang Su-Yan, Liu Jing-Hua. Determination of Six Trace Elements in Horseradish Tree Leaves by Inductively coupled Plasma-Atomic Emission Spectrometry. Chinese Journal of Spectroscopy Laboratory, 2005, 22(5): 1102-1104.

Google Scholar

[6] Wan Yi-qun, Xiao Li-feng, Liu Ying-xia, Huang Zi-juan. Spectroscopy and Spectral Analysis, 2008, 28(9): 2177-2180.

Google Scholar

[7] Zhang Sheng-bang, Sun Pei-long. Simultaneous determination of trace elements in Evodia rutaecarpa (Juss. ) Benth by ICP-AES. Journal of ZheJiang University of Technology, 2006, 34(1): 43-44, 55.

Google Scholar

[8] Fu Zhi-hong, Xie Ming-yong, Zhang Zhi-ming, Guo Lan. Spectroscopy and Spectral Analysis, 2004, 24 (6): 737-740.

Google Scholar

[9] He Jin-zhe, Kui Xiao-yun, Yang Kai, Shao Pin, Sun Pei-long. Analysis of Twenty Trace Elements in LingZhi by ICP-AES. Spectroscopy and Spectral Analysis. 2009, 29(5): 1409-1421.

Google Scholar

[10] Hirotaka Matsuura, Akiko Hokura, Fumie Katsuki, Akihide Itoh, Hiroki Haraguchi. Multielement Determination and Speciation of Major-to-Trace Elements in Black Tea Leaves by ICP-AES and ICP-MS with the Aid of Size Exclusion Chromatography. Analytical sciences, 2001, 17(3): 391-398.

DOI: 10.2116/analsci.17.391

Google Scholar

[11] Stephanie de Villiers, Mervyn Greaves, Henry Elderfield. An intensity ratio calibration method for the accurate determination of Mg/Ca and Sr/Ca of marine carbonates by ICP-AES. Geochemistry, Geophysics and Geosystems. 2002, 3(1).

DOI: 10.1029/2001gc000169

Google Scholar

[12] Liu Yanyan. Determination of Twenty-six Elements in Three Three Traditional Chinese Medicines Digested by Microwave and Determined by ICP-MS. Journal of Tongren Vocational and Technical College(Natural Science Edition). 2010, 8(5): 55-57.

Google Scholar

[13] Maximum levels of contaminants in foods. Inspection and Quarantine of the People's Republic of China, GB2762-(2012).

Google Scholar

[14] Ning Pengbo, Gong Chunmei, Zhang Yanming, Guo Kangkang. Analysis of Rare Earth Elements in Pu'er Tea of Yunnna by ICP-AES. Spectroscopy and Spectral Analysis. 2010, 30(10): 2830-2833.

Google Scholar

[15] Rui Yukui, Hao Yanling, Zhang Fusuo, Jin Yinhua, GuoJing. Application of ICP-MS/ICP-AES to Detection of 22 Trace Elements in Fruits of Elm. Spectroscopy and Spectral Analysis. 2007, 27 (10): 2111-2113.

Google Scholar