Production of Zirconium Diboride Powder by Self Propagating High Temperature Synthesis

Burcu Akkas; Murat Alkan; Bora Derin; Yücel Onüralp

doi:10.4028/www.scientific.net/AST.63.251

Paper Titles

Macrokinetics for Macrostructure Forming of a Product in Self-Propagating High-Temperature Synthesis
p.222

Past and Current Accomplishments in Production of Ceramic Powders and Structures by Self-Propagating High-Temperature Synthesis Method
p.228

Carbon Combustion Synthesis of Ceramic Oxide Nanopowders
p.236

Double SHS of W₂B₅ Powder from CaWO₄ and B₂O₃
p.246

Production of Zirconium Diboride Powder by Self Propagating High Temperature Synthesis
p.251

Utilization of NbC Nanoparticles Obtained by Reactive Milling in Production of Alumina Niobium Carbide Nanocomposites
p.257

Composites Produced by SHS Method – Current Development and Future Trends
p.263

Self-Propagating High-Temperature Synthesis of Iron- and Copper-Matrix Cermets
p.273

Sintering and Hot-Pressing of Ti₂AlC Obtained by SHS Process
p.282

HomeAdvances in Science and TechnologyAdvances in Science and Technology Vol. 63Production of Zirconium Diboride Powder by Self...

Production of Zirconium Diboride Powder by Self Propagating High Temperature Synthesis

Abstract:

In this study, the self-propagating high-temperature synthesis (SHS) and following acid leaching techniques were carried out to produce zirconium diboride (ZrB2) powder. In the SHS experiments, technical grade ZrO2 powder, and different amounts of B2O3 and Mg powders were used. The SHS products were obtained in the form of black, spongy solid. In the leaching step, the effect of different acid concentrations on selective leaching was investigated by using optimum SHS product to eliminate the impurities such as MgO, Mg3B2O6 and Mg2B2O5. The products obtained were characterized by using XRD, ICP and SEM techniques.

You might also be interested in these eBooks

12th INTERNATIONAL CERAMICS CONGRESS PART B

View Preview

Info:

Periodical:

Advances in Science and Technology (Volume 63)

Pages:

251-256

DOI:

https://doi.org/10.4028/www.scientific.net/AST.63.251

Citation:

Cite this paper

Online since:

October 2010

Authors:

Burcu Akkas, Murat Alkan, Bora Derin, Yücel Onüralp

Keywords:

HCI Leaching, SHS Process, Zirconium Diboride Powder

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

References

[1] N. Setoudeh and N.J. Welham: Journal of Alloys and Compounds 420 (2006), pp.225-228.

Google Scholar

[2] S.K. Mishra, S. Das and L.C. Pathak: Materials Science and Engineering A364 (2004), pp.249-255.

Google Scholar

[3] H.E. Çamurlu and F. Maglia: Journal of the European Ceramic Society 29 (2009), pp.1501-1506.

Google Scholar

[4] S. Zhu, W.G. Fahrenholtz, G.E. Hilmas and S.C. Zhang: Materials Science and Engineering A459 (2007), pp.167-171.

Google Scholar

[5] A.K. Khanra, L.C. Pathak and M.M. Godkhindi: Journal of Materials Processing Technology 202 (2008), pp.386-390.

DOI: 10.1016/j.jmatprotec.2007.09.007

Google Scholar

[6] S.K. Mishra, S. Das, R.P. Goel and P.R. Rao, U.S. Patent US2004/0022712A1 (2004).

Google Scholar

[7] F. Habashi, in: Handbook of Extractive Metallurgy, Vol. IV Weinheim, Wiley-VCH Germany (1997), p.1452.

Google Scholar

[8] A.W. Weimer, in: Thermochemistry and kinetics in Carbide, Nitride, and Boride Materials Synthesis and Processing, Chapman & Hall, London, England (1997), pp.79-114.

DOI: 10.1007/978-94-009-0071-4_3

Google Scholar

[9] H.H. Nersisyan, J.H. Lee, and C.W. Won, Combustion and Flame: 142 (2005), pp.241-248.

Google Scholar

[10] O. Yücel, F.Ç. Şahin and A. Tekin: High temperature Materials and processes 15 (1996), pp.103-109.

Google Scholar

[11] S. Yazıcı: Production of Tungsten Boride Powder via Self Propagating High-Temperature Synthesis, M.S. Thesis, Istanbul Technical University, Istanbul (2009), pp.82-85.

Google Scholar