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Effect of Lanthanum Substitution on Structure and Modulation in Bi2Sr2-xLaxCaCu2O8+d (0≤x≤0.3) Superconducting Compound

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Abstract:

The effect of La substitution on the structure and its modulation in samples with a nominal composition of Bi2Sr2-xLaxCaCu2O8+d where 0≤x≤0.3 superconducting phase was investigated. The X-ray powder diffraction (XRPD) results showed an almost pure Bi-2212 phase, confirmed by the estimated amount of element concentration using dispersive energy X-ray spectroscopy (EDX). Scanning electron microscopy (SEM) micrographs showed a decrease of both crystallite size and connectivity when Lanthanum concentration increases. Le Bail refinement using the Jana2006 program gives a very good value of goodness of fit (GOF) factor. Also, the refinement reveals that for x=0.3 the orthorhombic cell transforms to the tetragonal one and the modulation vector q increases when increasing La concentration.

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Periodical:

Defect and Diffusion Forum (Volume 406)

Pages:

240-249

DOI:

https://doi.org/10.4028/www.scientific.net/DDF.406.240

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Online since:

January 2021

Authors:

Mourad Mimouni*, Mohammed Sadok Mahboub, Mohammed Fayçal Mosbah, Ghani Rihia, Soraya Zeroual, Mebrouk Ghougali, Azzeddine Beggas

Keywords:

Bi Based Superconductors, Bi-2212, Doping, Jana2006, Modulated Structure

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