Optimization of Sidoarjo Mud Akaline Fusion Process Using Taguchi Method

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Sidoarjo mud contains 48.3% silica which is considered as the biggest impurity when compared to the content of rare earth metals which are 0.3% Eu and 0.02% Yb. The hydrothermal process is used to bind silica as a form of silica extraction activity in the Sidoarjo mud so that the Rare Earth Elements are purified further because their uses are urgently needed. This process compares the alkalis in the form of Na2CO3 and K2CO3 which are basic salts which will then be compared to the most optimum conditions of the two alkalis. Each alkali will be processed under operating conditions following the Taguchi method which aims to minimize research and optimize research results. Based on the research results, it was found that K2CO3 provided better silica recovery than Na2CO3 under operating conditions with a K2CO3 concentration of 2 M, 1 hour soaking time, 700°C melting temperature and 3 hours melting time, giving 95.24% silica recovery. In addition, by using the Taguchi method it can be analyzed that the main factors affecting the melting of the alkali are the melting time, the concentration of the alkali, the temperature of the melting, and the immersion time.

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December 2024

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[1] Adinda R H P, Adam D L. Analisis Potensi dan Arah Strategi Kebijakan Logam Tanah Jarang di Indonesia. Prosiding TPT XXXI PERHAPI. 2022; 105 -106

Google Scholar

[2] Ibrahim, I. A. M., Zikry, A. A. F., Sharaf, M. A., & Zikry, A. Preparation of spherical silica nanoparticles: Stober silica. In Journal of American Science. 2010; 6 (11)

Google Scholar

[3] Todkar, B. S., Deorukhkar, O. A., & Deshmukh, S. M. Extraction of Silica from Rice Husk. In International Journal of Engineering Research. 2016.; 12 (3)

Google Scholar

[4] Suprapto, S. J. Tinjauan Tentang Unsur Tanah Jarang. Buletin Sumber Daya Geologi. 2009; 4 (1); 36–47

DOI: 10.47599/bsdg.v4i1.173

Google Scholar

[5] Sawolo N, Sutrisno E, Istadi B P, Darmoyo A B. The LUSI mud volcano triggering controversy: Was it caused by drilling?. Marine and Petroleum Geology. 2009; 1766–1784

DOI: 10.1016/j.marpetgeo.2009.04.002

Google Scholar

[6] Anom Wiryasa, Ngk., & Sudarsana, I. Pemanfaatan Lumpur Lapindo Sebagai Bahan Substitusi Semen Dalam Pembuatan Bata Beton Pejal. Jurnal Ilmiah Teknik Sipil. 2009; 13 (1); 39–46.

DOI: 10.55114/siparstika.v1i1.265

Google Scholar

[7] Sulistiyono Eka, S. D. Pemurnian Zirkon untuk Bahan Dasar Refraktori Berbasis Zirkonia. (1996)

Google Scholar

[8] Lester L. Knapp, Morton Smutz, F. H. Solvent Extraction Equilibria for Rare E. 1956; 132

Google Scholar

[9] Mirmohamadsadeghi, S., & Karimi, K. Recovery of silica from rice straw and husk. In Current Developments in Biotechnology and Bioengineering: Resource Recovery from Wastes. 2020; 411–433

DOI: 10.1016/b978-0-444-64321-6.00021-5

Google Scholar

[10] Abdelkader, A. M., Daher, A., & El-kashef, E. Novel decomposition method for zircon. 2008; 460; 577–580

DOI: 10.1016/j.jallcom.2007.06.032

Google Scholar

[11] Prameswara, G., Logam, P., Jarang, T., Erak, D. T., Dengan, T. I., Klorida, A., Elah, S. E. T., & Fu, P. Ekstraksi Logam Tanah Jarang dan Logam Berharga dari Produk Fusi Alkaline Tailing Zirkon. (2019)

DOI: 10.17146/eksplorium.2016.37.1.2719

Google Scholar

[12] Guan, W., Lv, H., Zirconia, N. C., Zhang, L., Liu, T., Mccormick, L. D., & Wheeler, N. S. Primary study of KOH alkaline fusion – nitric acid leaching process in extraction of West Kalimantan zircon concentrate Primary study of KOH alkaline fusion – nitric acid leaching process in extraction of West Kalimantan zircon concentrate. (2020)

DOI: 10.1088/1757-899x/763/1/012065

Google Scholar

[13] Wira D, Mauritz P M. Analysis Of The Types And Levels Of Akar Kuning (Fibraurea chloroleuca Miers) Extract By Gravimetric. Jurnal Pendidikan Kimia dan Ilmu Kimia. 2020; 3

DOI: 10.31602/dl.v3i1.3109

Google Scholar

[14] Hayat K, Aditya S, Adrien D, Terry L A, Daria C B, Gregory S P. Experimental methods in chemical engineering: X-ray diffraction spectroscopy—XRD. The Canadian Journal of Chemical Engineering. (2019)

Google Scholar

[15] G Zadora, Brozek M Z. SEM–EDX—a useful tool for forensic examinations. Materials Chemistry and Physics 81. 2003; 345 - 348

DOI: 10.1016/s0254-0584(03)00018-x

Google Scholar

[16] Sulistiyono Eka, S. D. Pemurnian Zirkon untuk Bahan Dasar Refraktori Berbasis Zirkonia. (1996)

Google Scholar

[17] Guan, W., Lv, H., Zirconia, N. C., Zhang, L., Liu, T., Mccormick, L. D., & Wheeler, N. S. Primary study of KOH alkaline fusion – nitric acid leaching process in extraction of West Kalimantan zircon concentrate Primary study of KOH alkaline fusion – nitric acid leaching process in extraction of West Kalimantan zircon concentrate. (2020)

DOI: 10.1088/1757-899x/763/1/012065

Google Scholar

[18] Bambang Wahyudi, Srie Muljani. Pupuk Multinutrient Berbasis Silika Dari Limbah Geothermal Sludge Dengan Proses Asidifikasi. Jurnal Teknik Kimia. 2019; 14 (1); 22 - 27

DOI: 10.33005/jurnal_tekkim.v14i1.1651

Google Scholar

[19] Biao Liu, et all. A Novel Method to Extract Vanadium and Chromium from Vanadium Slag using Molten NaOH-NaNO3 Binary System. Wiley Online Library. (2020)

DOI: 10.1016/j.jhazmat.2019.120805

Google Scholar

[20] Fei Liu , Xiao Dan Wang, Jian Xin Cao. Effect of Hydrothermal Process on Xonotlite Crystal. Advanced Materials Research. 2012; 382; 379-383.

DOI: 10.4028/www.scientific.net/amr.382.379

Google Scholar

[21] Muhammad Nurhasan Assidiq. Metode Taguchi Multi Respon Untuk Mencari Kombinasi Level Faktor Optmal Dalam Perbaikan Kualitas Keramik Tradisional. Jurnal Industrikrisna. 2023; 12 (1); 69-83.

DOI: 10.61488/industrikrisna.v12i1.218

Google Scholar

[22] Annisa Ayu Wulandari, Triastuti Wuryandari, Dwi Ispriyanti. Penerapan Metode Taguchi Untuk Kasus Multirespon Menggunakan Pendekatan Grey Relational Analysis Dan Principal Component Analysis (Studi Kasus Proses Freis Komposit GFRP). Jurnal Gaussian. 2016; 5 (4); 791 – 800.

Google Scholar

[23] Erlinda Ningsih, Sri Rachmania Juliastuti, Raden Darmawan, Nuniek Hendrianie, Orchidea Rachmaniah. Initial extraction of sodium silicate from sidoarjo mud by alkaline fusion and water leaching. Heliyon. 2023; 9 (6)

DOI: 10.1016/j.heliyon.2023.e17095

Google Scholar