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HomeJournal of Nano ResearchJournal of Nano Research Vol. 53Rattle-Type Diamine-Functionalized Mesoporous...

Rattle-Type Diamine-Functionalized Mesoporous Silica Sphere for Carbon Dioxide Adsorption

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Abstract:

A rattle-type diamine-functionalized mesoporous silica sphere (DA-RMSS) was fabricated stepwise using a self-templating method through cationic surfactant assisted selective etching strategy. The rattle-type morphology of the obtained DA-RMSS material was disclosed by transmission electron microscopy, while its chemical composition was characterized by CHN elemental analysis, Fourier transform infrared spectroscopy, and solid-state ²⁹Si cross-polarization/magic-angle-spinning nuclear magnetic resonance spectroscopic measurement, which corroborates the successful formation of siloxane network and the incorporation of organic component. Moreover, nitrogen adsorption–desorption isotherm measurement was conducted to reveal that DA-RMSS possesses large Brunauer–Emmett–Teller (BET) specific surface area of 814 m²g^–1, pore volume of 0.78 cm³g^–1, and narrow pore size distribution centered at 3.0 nm. Furthermore, its uptake property on carbon dioxide was also investigated in this contribution.

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Journal of Nano Research Vol. 53

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Periodical:

Journal of Nano Research (Volume 53)

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13-21

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https://doi.org/10.4028/www.scientific.net/JNanoR.53.13

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Online since:

June 2018

Authors:

Ning Yuan*, Zhi Wei Liu, Li Yan Wang, Bao Hang Han

Keywords:

Carbon Dioxide Adsorption, Mesoporous Silica, Rattle-Type Structure, Self-Templating, Yolk-Shell Structure

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© 2018 Trans Tech Publications Ltd. All Rights Reserved

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