Innovative 3D-Printed Tantalum Patches for Non-Destructive Repair of Enamelled Reactors

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Glass-enamel coated reactors are essential in chemical and pharmaceutical production, yet repairing local enamel defects remains difficult without risking further damage. This work introduces a non-destructive repair concept using a custom 3D-printed tantalum patch that magnetically adheres to the curved reactor surface. The patch, produced by powder bed fusion and equipped with a silicone gasket and embedded neodymium magnets, was tested in a glass-lined laboratory reactor under 18 combinations of temperature, pressure, and mixing speed. A pH-indicator paper placed beneath the patch verified sealing performance in a mildly acidic medium. No liquid penetration occurred under any tested condition, demonstrating that the magnetically fixed tantalum patch provides effective temporary repair of enamel defects. The results support its potential industrial applicability and highlight future development needs in gasket optimization and magnetic clamping design.

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61-69

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July 2026

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© 2026 Trans Tech Publications Ltd. All Rights Reserved

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[1] K. Xu, "Improving the mechanical impact and bending resistances of enamel coatings by B₂O₃ addition," Surf. Coat. Technol., 2021

DOI: 10.1016/j.ceramint.2021.06.140

Google Scholar

[2] E. Medvedovski, G. Leal Mendoza, "Enamel (glassy) coatings for steel protection against high temperature corrosion," Adv. Appl. Ceramics, 2023

DOI: 10.1080/17436753.2023.2231699

Google Scholar

[3] "The Complete Guide to Glass‑Lined Reactor Repair: What Every Plant Should Know," Glasskem, 2024. [Online, 2025.11.27.]. Available: https://glasskem.ca/the-complete-guide-to-glass-lined-reactor-repair-what-every-plant-should-know/

DOI: 10.4159/9780674984189-009

Google Scholar

[4] "Failure and repair of glass-lined reactor", Kaizhi Chemical Equipment, 2021. [Online,2025.11.27.]. Available: https://en.kztbl.com/news/5.html

Google Scholar

[5] "Belzona Simplifies Repairs in Glass Lined Reactors", Belzona Case Study, 2025. [Online,2025.11.27.].Available: https://khia.belzona.com/khia/BELZONA_SIMPLIFIES_REPAIRS_IN_GLASS_LINED_REACTORS

Google Scholar

[6] A. A. A. Aliyu, K. Poungsiri, J. Shinjo, C. Panwisawas, R. C. Reed, C. Puncreobutr, K. Tumkanon, S. Kuimalee, B. Lohwongwatana, "Additive manufacturing of tantalum scaffolds: processing, microstructure and process‑induced defects," Int. J. Refractory Metals Hard Mater., vol. 112, 106132, 2023

DOI: 10.1016/j.ijrmhm.2023.106132

Google Scholar

[7] A. U. H. Mohsan, D. Wei, "Advancements in Additive Manufacturing of Tantalum via the Laser Powder Bed Fusion (PBF‑LB/M): A Comprehensive Review," Materials, vol. 16, no. 19, 6419, 2023

DOI: 10.3390/ma16196419

Google Scholar

[8] "Reglass Your Equipment with Our DD3009 Enamel," De Dietrich Process Systems, 2024. [Online, 2025.11.27.]. Available: https://www.dedietrich.com/en/resources/reglass-your-equipment-our-dd3009-enamel

Google Scholar

[9] "Preventive Maintenance for Glass‑Lined Reactors," Glasskem Inc., 2024. [Online, 2025.11.27.]. Available: https://glasskem.ca/the-role-of-preventive-maintenance-in-extending-thelife-of-glass-lined-reactors/

Google Scholar

[10] S. D. Proell et al., "A highly efficient computational approach for fast scan-resolved microstructure predictions in metal additive manufacturing on the scale of real parts," Addit. Manuf., vol. 92, 104380, 2024

DOI: 10.1016/j.addma.2024.104380

Google Scholar

[11] 'Water - Density, Specific Weight and Thermal Expansion Coefficients'. Accessed: Nov. 17, 2023. [Online, 2025.11.27.]. Available: https://www.engineeringtoolbox.com/water-density-specific-weight-d_595.html

Google Scholar

[12] 'Water - Dynamic (Absolute) and Kinematic Viscosity vs. Temperature and Pressure'. Accessed: Nov. 17, 2023. [Online, 2025.11.27.]. Available: https://www.engineeringtoolbox.com/water-dynamic-kinematic-viscosity-d_596.html

Google Scholar

[13] Z. Pálfi, Chemical Industry Equipment – Design Atlas. Budapest: Műszaki Könyvkiadó, 1986. ISBN: 963106249X, 9789631062496

Google Scholar

[14] De Dietrich, Products Portfolio – Glass-Lined Technology & Other Materials. De Dietrich Process Systems. [Online, 2025.11.27.]. Available: https://pdf.directindustry.com/viewerCatalog/de-dietrich/product-portofolio-catalog/161798-657055.html#open

Google Scholar